Simultaneous Determination of 15 Plant Growth Regulators in Bean Sprout and Tomato with Liquid Chromatography–Triple Quadrupole Tandem Mass Spectrometry
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- 作者：Liyan Ma (1) (3)
Hongyan Zhang (2) (3)
Wentao Xu (1) (3)
Xiaoyun He (1) (3)
Lili Yang (1)
Yunbo Luo (1)
Kunlun Huang (1) (3) - 关键词：Plant growth regulator ; Bean sprout ; Tomato ; LC ; MS/MS
- 刊名：Food Analytical Methods
- 出版年：2013
- 出版时间：June 2013
- 年：2013
- 卷：6
- 期：3
- 页码：941-951
- 全文大小：488KB
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Hongyan Zhang (2) (3)
Wentao Xu (1) (3)
Xiaoyun He (1) (3)
Lili Yang (1)
Yunbo Luo (1)
Kunlun Huang (1) (3)
1. College of Food Science and Nutritional Engineering, China Agricultural University, Beijing, 100083, People’s Republic of China
3. Supervision and Testing Center of Agricultural Products Quality, Ministry of Agriculture, Beijing, 100083, People’s Republic of China
2. College of Science, China Agricultural University, Beijing, 100193, People’s Republic of China - ISSN：1936-976X
文摘
The present paper describes the development and validation of a new reversed-phase liquid chromatography–electrospray ionization tandem mass spectrometric method for determination of 15 plant growth regulators in bean sprout and tomato. Plant growth regulators were extracted with mixed solvents methanol/acetonitrile/water/acetic acid (v/v/v/v, 40/40/20/1) from 10?g vegetable and analyzed directly without further cleanup. The identification of each analyte was established by chromatographic retention time, analyte-specific fragmentation patterns, and relative peak area ratios of precursor/product ion pairs. The recoveries of 15 plant growth regulators in bean sprout and tomato were 70.3-10.0?%. The repeatability of this method is excellent, and relative standard deviation value is less than 10?%.