Polyol-mediated syntheses of crystalline nanosized manganese oxides
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- 作者：Guiqiang Diao (1) (2)
Fran?ois Chau (1)
Jean-Yves Piquemal (1)
Emmanuel Briot (5)
Souad Ammar (1)
Micka?l Sicard (4)
Sophie Nowak (1)
Patricia Beaunier (3)
Hélène Lecoq (1)
P. Decorse (1)
Lin Yu (2) - 关键词：Manganese oxide ; Polyol ; Synthesis ; Birnessite ; Spinel ; Nanoflake
- 刊名：Journal of Nanoparticle Research
- 出版年：2014
- 出版时间：June 2014
- 年：2014
- 卷：16
- 期：6
- 全文大小：
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Fran?ois Chau (1)
Jean-Yves Piquemal (1)
Emmanuel Briot (5)
Souad Ammar (1)
Micka?l Sicard (4)
Sophie Nowak (1)
Patricia Beaunier (3)
Hélène Lecoq (1)
P. Decorse (1)
Lin Yu (2)
1. Université Paris Diderot, Sorbonne Paris Cité, ITODYS, CNRS UMR 7086, 15 rue J.-A. de Ba?f, 75205, Paris Cedex 13, France
2. Faculty of Chemical Engineering and Light Industry, Guangdong University of Technology, Guangzhou, 510006, People’s Republic of China
5. UPMC-Paris 06, UMR 8234, Laboratoire de Physicochimie des Electrolytes et Nanosystèmes Interfaciaux, Sorbonne Universités, 4 Place Jussieu, 75005, Paris, France
4. Department of Fundamental and Applied Energetics, ONERA, 91761, Palaiseau Cedex, France
3. UPMC-Paris 06, UMR 7197, Laboratoire de Réactivité de Surface, Sorbonne Universités, 4 Place Jussieu, 75005, Paris, France - ISSN：1572-896X
文摘
Potassium-type birnessite and lithium-containing manganese oxides were prepared by the polyol process. The Mn(III)/Mn(IV) mixed-valencies compounds are obtained through the controlled reduction of potassium permanganate in a basic water–diethylene glycol mixture at moderate temperature and very short reaction time, 70?°C and 10?min, respectively. Both solids are quite well crystallized and display high specific surface areas, 137 and 329?m2?g?, respectively. Several polyols with variable chain lengths have been used and it is shown that the nature of the polyol has a marked influence on the textural properties of the birnessite-type solid.