Salt-Assisted Graphene Oxide Dispersive Solid Phase Microextraction for Sensitive Detection of Malachite Green and Crystal Violet by HPLC
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- 作者：Gongheng Li ; Xinfeng Zhang ; Leilei Zhang ; Shuxia Xu ; Chongying Li
- 关键词：High ; performance liquid chromatography ; Graphene ; Dispersive solid phase microextraction ; Malachite green ; Crystal violet
- 刊名：Chromatographia
- 出版年：2015
- 出版时间：August 2015
- 年：2015
- 卷：78
- 期：15-16
- 页码：979-985
- 全文大小：975 KB
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Xinfeng Zhang (1) (2)
Leilei Zhang (1)
Shuxia Xu (1) (2)
Chongying Li (1) (2)
1. College of Material and Chemistry and Chemical Engineering, Chengdu University of Technology, Chengdu, 610059, People’s Republic of China
2. Mineral Resources Chemistry Key Laboratory of Sichuan Higher Education Institutions, Chengdu University of Technology, Chengdu, 610059, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Analytical Chemistry
Organic Chemistry
Pharmacy
Biochemistry
Plant Sciences
Measurement Science and Instrumentation - 出版者：Vieweg Verlag
- ISSN：1612-1112
文摘
In this study, an efficient sample pretreatment method, salt-assisted graphene oxide dispersive solid phase microextraction (SA-GO-DSPME), was established for extraction of malachite green (MG) and crystal violet (CV). The dispersive graphene oxide was found to be easily aggregated and completely centrifuged in the presence of NaCl. The adsorption kinetic of SA-GO-DSPME was shown to be quite fast (equilibrium time?=?5?min). Key parameters that influenced extraction efficiency including sample pH, the eluent type, GO amount, extraction time, NaCl concentration and centrifuging time were investigated. Coupled with SA-GO-DSPME, high-performance liquid chromatography (HPLC) could be used for sensitive detection of MG and CV with detection limits down to 1.7 and 0.3?ng?mL? for MG and CV, respectively. The relative standard deviations for extraction reproducibility (n?=?5) were 1.8?% for MG and 3.8?% for CV. The proposed method has been successfully applied for detection of MG and CV in real water samples, and the recoveries ranged from 89.7 to 116.4?%. This simple and fast extraction method may provide a promising alternative for extraction of trace amount of MG and CV in complicated samples.