Synthesis, spectral, antimicrobial, and thermal properties of Ce(III), Gd(III), Nd(III), Tb(III), and Er(III) gliclazide complexes

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• 作者：M. G. Abd El-Wahed ; S. M. El-Megharbel…
• 关键词：gliclazide ; lanthanides ; complexes ; antimicrobial activity
• 刊名：Russian Journal of General Chemistry
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：86
• 期：2
• 页码：391-399
• 全文大小：392 KB
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• 作者单位：M. G. Abd El-Wahed (1)
  S. M. El-Megharbel (1) (2)
  M. Y. El-Sayed (1)
  Y. M. Zahran (1)
  M. S. Refat (2) (3)
  M. A. Al-Omar (4)
  A. M. Naglah (4) (5)
  
  1. Department of Chemistry, Faculty of Science, Zagazig University, Zagazig, Egypt
  2. Department of Chemistry, Faculty of Sciences, Taif University, Al-Haweiah, P.O. Box 888, Taif, 21974, Saudi Arabia
  3. Department of Chemistry, Faculty of Science, Port Said University, Port Said, Egypt
  4. Department of Pharmaceutical Chemistry, Drug Exploration & Development Chair, College of Pharmacy, King Saud University, Riyadh, 11451, Saudi Arabia
  5. Peptide Chemistry Department, Chemical Industries Research Division, National Research Centre, Dokki, Cairo, 12622, Egypt
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Chemistry
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1608-3350

文摘

The complexation between the lanthanide metal ions Ce(III), Gd(III), Nd(III), Tb(III), and Er(III) and gliclazide produced 1 : 1 molar ratio metal: gliclazide (Glz) complexes coordinated in a monodentate fashion via the OH group and having the general formulas [M(Glz)Cl₃(H₂O)]·xH₂O (M = Ce, Gd, Nd and x = 1, 3, 4, respectively) and [M(Glz)(H₂O)₄]Cl₃·yH₂O (M = Tb, Er and y = 1, 2, respectively). The structure of the synthesized lanthanide gliclazide complexes was assigned by IR, 1HNMR, and UV-Vis spectroscopy. Thermal analysis and kinetic and thermodynamic parameters gave evidence for the thermal stability of the Glz complexes. The latter showed a significant antimicrobial effect against some bacteria and fungi.