参考文献:1. Ahmad M, Siddiqui HL, Zia-ur-Rehman M, Parvez M (2010) Anti-oxidant and antibacterial activities of novel / N鈥?arylmethylidene-2-(3,4-dimethyl-5,5-dioxidopyrazolo[4,3- / c][1,2]benzothiazin-2(4 / H)-yl) acetohydrazides. Eur J Med Chem 45:698鈥?04 CrossRef 2. Ahmad N, Rehman MZ, Siddiqui HL, Fasih Ullah M, Parvez M (2011) Microwave assisted synthesis and structure鈥揳ctivity relationship of 4-hydroxy- / N鈥?[1-phenylethylidene]-2H/2-methyl-1,2-benzothiazine-3-carbohydrazide 1,1-dioxides as anti-microbial agents. Eur J Med Chem 46:2368鈥?377 CrossRef 3. Altomare A, Cascarano G, Giacovazzo C, Guagliardi A (1993) Completion and refinement of crystal structures with SIR92. JAppl Cryst 26:343鈥?50 CrossRef 4. Baraldi PG, Manfredini S, Romagnoli R, Stevanato L, Zaid AN, Manservigi R (1998) Synthesis and anti-HSV-1 activity of 6 substituted pyrazolo[3,4-d]pyridazin-7-one nucleosides. Nucleosides Nucleotides 17(12):2165鈥?171 CrossRef 5. Beurskens PT, Admiraal G, Beurskens G, Bosman WP, de Gelder R, Israel R, Smits JMM (1994) The / DIRDIF- / 94 program system. Technical Report of the Crystallography Laboratory, University of Nijmegen, Nijmegen 6. Boger DL, Miyazaki S, Kim SH, Wu JH, Castle SL, Loiseleur O, Jin Q (1999) Total synthesis of the vancomycin aglycon. J Am Chem Soc 121:10004鈥?0011 CrossRef 7. Braughler JM, Duncan LA, Chase RL (1986) The involvement of iron in lipid peroxidation. Importance of ferric to ferrous ratios in initiation. J Biol Chem 261:10282鈥?0289 8. Bruno O, Bondavalli F, Ranise A, Schenone P, Losasso C, Cilenti L, Matera C, Marmo E (1990) 3,5-Diphenyl-1 / H-pyrazole derivatives. V鈥?-acetyl-4-hydroxy-3,5-diphenyl-2-pyrazoline esters, 4-hydroxy-3,5-diphenyl-1 / H-pyrazole esters and / N-substituted 4-(3-amino-2-hydroxy-1-propoxy)-1-methyl-3,5-diphenyl-1 / H-pyrazoles with antiarrhythmic, sedative and platelet antiaggregating activities. Farmaco 45(2):147鈥?66 9. Cottineau B, Toto P, Marot C, Pipaud A, Chenault J (2002) Synthesis and hypoglycemic evaluation of substituted pyrazole-4-carboxylic acids. Bioorg Med Chem Lett 12:2105鈥?108 CrossRef 10. Cremer D, Pople JA (1975) General definition of ring puckering coordinates. J Am Chem Soc 97:1354鈥?358 CrossRef 11. Farrugia LJ (1997) ORTEP-3 for windows鈥攁 version of ORTEP-III with a graphical user interface (GUI). J Appl Cryst 30:565 CrossRef 12. Foroumadi A, Samzadeh-Kermani A, Emami S, Dehghan G, Sorkhi M, Arabsorkhi F, Heidari MR, Abdollahi M, Shafiee A (2007) Synthesis and antioxidant properties of substituted 3-benzylidene-7-alkoxychroman-4-ones. Bioorg Med Chem Lett 17:6764鈥?769 CrossRef 13. Gaulejac NSC, Glories Y, Vivas N (1999) Free radical scavenging effect of anthocyanins in red wines. Food Res Int 32:327鈥?33 CrossRef 14. Giuseppe M, Arnaldo F, Patrizia T (1987) Derivatives of pyrido-benzothiazine with high anti-microbial activity. US Patent 4,668,784, 26 May 1987 15. Gutteridge JMC (1993) Free radicals in disease processes: a compilation of cause and consequence. Free Radic Res Commun 19:141鈥?58 CrossRef 16. Hooft R (1998) Collect. Nonius BV, Delft 17. Huang Z, Reilly JR, Buckle RN (2007) An efficient synthesis of amides and esters via triacyloxyboranes. Synlett 7:1026鈥?030 CrossRef 18. Ikeda T, Kakegawa H, Miyataka H, Matsumoto H, Satoht T (1992) Anti-allergic and anti-inflammatory actions of 2鈥?(tetrazole-5-yl)-4-hydroxy-2-methyl-2 / H-1,2-benzothiazine-3-carboxanilide 1,1-dioxide. Bioorg Med Chem Lett 2:709鈥?14 CrossRef 19. Iovu M, Zalaru C, Dumitrascu F, Draghici C, Moraru M, Criste E (2003) New substituted 2-(pyrazol-1-yl)-dialkylacetanilides with potential local anesthetic and antiarrhythmic action. Part II. IL Farmaco 58:301鈥?07 CrossRef 20. Krapcho J, Somerset NJ (1968) Therapeutically active benzothiazines. US Patent 3, 401,166, 10 Sept 1968 21. Krapcho J, Somerset NJ (1969) Hydroxyalkylene-substituted benzoxazines and benzothiazines. US Patent 3,459,748, 5 Aug 1969 22. Krapcho J, Somerset NJ (1969) Substituted benzoxazines and benzothiazines. US Patent 3,455,915, 15 July 1969 23. Lomabardino JG, Wiseman ED (1972) Sudoxicam and related / N-heterocyclic carboxamides of 4-hydroxy-2 / H-1,2-benzothiazine 1,1-dioxide. Potent nonsteroidal antiinflammatory agents. J Med Chem 15:848鈥?49 CrossRef 24. Lomabardino JG, Wiseman EH, McLamore WM (1971) Synthesis and antiinflammatory activity of some 3-carboxamides of 2-alkyl-4-hydroxy-2 / H-1,2-benzothiazine 1,1-dioxide. J Med Chem 14:1171鈥?175 CrossRef 25. Lombardino JG, Wiseman EH, Chiaini J (1973) Potent antiinflammatory / N-heterocyclic 3-carboxamides of 4-hydroxy-2-methyl-2 / H-1,2-benzothiazine 1,1-dioxide. J Med Chem 16:493鈥?96 CrossRef 26. Otwinowski Z, Minor W (1997) Processing of X-ray diffraction data collected in oscillation mode. Methods Enzymol 276:307鈥?26 CrossRef 27. Riyadh SM (2011) Enaminones as building blocks for the synthesis of substituted pyrazoles with antitumor and antimicrobial activities. Molecules 16:1834鈥?853 CrossRef 28. Shaheen F, Ahmad M, Khan MTH, Jalil S, Ejaz A, Sultankhodjaev MN, Arfan M, Choudhary MI, Rahman A (2005) Alkaloids of aconitum laeve and their anti-inflammatory, antioxidant and tyrosinase inhibition activities. Phytochemistry 66:935鈥?40 CrossRef 29. Sheehan JC, Hess GP (1955) A new method of forming peptide bonds. J Am Chem Soc 77:1067鈥?068 CrossRef 30. Sheldrick GM (2008) A short history of SHELX. Acta Cryst A64:112鈥?22 31. Silverstein FE, Faich G, Goldstein JL, Simon LS, Pincus T, Whelton A, Makuch R, Eisen G, Agrawal NM, Stenson WF, Burr AM, Zhao WW, Kent JD, Lefkowith JB, Verburg KM, Geis GS (2000) Gastrointestinal toxicity with celecoxib vs nonsteroidal anti-inflammatory drugs for osteoarthritis and rheumatoid arthritis: the CLASS study: a randomized controlled trial. J Am Med Assoc 284:1247鈥?255 CrossRef 32. Smith SR, Denhardt G, Terminelli C (2001) The anti-inflammatory activities of cannabinoid receptor ligands in mouse peritonitis models. Eur J Pharmacol 432:107鈥?19 CrossRef 33. Turck D, Busch U, Heinzel G, Narjes H, Nehmiz G (1995) Effect of food on the pharmacokinetics of meloxicam after oral administration. Clin Drug Invest 9:270鈥?76 CrossRef 34. Zia-ur-Rehman M, Choudary JA, Ahmad S, Siddiqui HL (2006) Synthesis of potential biologically active 1,2-benzothiazin-3-yl-quinazolin-4(3 / H)-ones. Chem Pharm Bull 54:1175鈥?178 CrossRef 35. Zinnes H, Lindo NA, Sircar JC, Schwartz ML, Shavel J Jr (1973) 1,2-Benzothiazines. 6. 3-Carbamoyl-4-hydroxy-2 / H-1,2-benzothiazine 1,1-dioxides as antiinflammatory agents. J Med Chem 16:44鈥?8 CrossRef
作者单位:Matloob Ahmad (1) (2) Hamid Latif Siddiqui (3) John M. Gardiner (4) Masood Parvez (5) Sana Aslam (3)
1. Institute of Chemistry, University of the Punjab, Lahore, 54590, Pakistan 2. Department of Chemistry, Govt. College University, Faisalabad, Pakistan 3. Institute of Chemistry, University of the Punjab, Lahore, 54590, Pakistan 4. School of Chemistry and Manchester Interdisciplinary Biocentre, University of Manchester, Manchester, M1 7DN, UK 5. Department of Chemistry, University of Calgary, 2500 University Drive N.W, Calgary, AB, T2N 1N4, Canada