Preparation of mixed matrix PES-based nanofiltration membrane filled with PANI-co-MWCNT composite nanoparticles
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- 作者：Ehsan Bagheripour ; Abdolreza Moghadassi…
- 关键词：Nanofiltration ; Membrane Fabrication/Characterization ; Mixed Matrix ; Polyaniline ; co ; multi Walled Carbon Nanotubes Composite Nanoparticles
- 刊名：Korean Journal of Chemical Engineering
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：33
- 期：4
- 页码：1462-1471
- 全文大小：2,392 KB
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Abdolreza Moghadassi (1)
Sayed Mohsen Hosseini (1)
1. Department of Chemical Engineering, Faculty of Engineering, Arak University, Arak, 38156-8-8349, Iran - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Industrial Chemistry and Chemical Engineering
Catalysis
Materials Science
Biotechnology - 出版者：Springer New York
- ISSN：1975-7220
文摘
Mixed matrix polyethersulfone/PANI-co-MWCNTs composite nanoparticle nanofiltration membrane was prepared by casting solution technique. Polyvinylpyrrolidone was also used as membrane pore former in membrane fabrication. The effect of polyaniline-co-multi walled carbon nanotubes composite nanoparticle concentration in the casting solution on membrane structure and performance was investigated. Scanning optical microscopy and scanning electron microscopy, FTIR analysis, porosity, mean pore size, contact angle, water content, NaCl/Na2SO4 rejection, water flux, tensile strength measurements and 3D surface image were also carried out in membrane characterization. SOM images showed nanoparticle agglomeration at high additive loading ratio. SEM images showed the membrane sub-layer porosity and thickness were changed by use of nanoparticles in membrane matrix. The membrane water content, porosity and pore size were increased by increase of nanoparticle concentration, except for 1%wt. Use of PANI-co- MWCNT nanoparticles in the membrane matrix caused a decrease of membrane contact angle from 63.43 to 46.76o. Salt rejection and water flux were improved initially by increase of nanoparticle concentration up to 0.1%wt and then decreased by more additive concentration. In addition, the membranes tensile strength was reduced by increase of PANI-co-MWCNTs composite nanoparticle concentration. 3D surface images showed a smoother surface for mixed matrix membrane filled with 0.1wt% PANI-co-MWCNTs. Modified membrane containing 0.1wt% composite nanoparticles showed better performance compared to others.