SO3H-modified petroleum coke derived porous carbon as an efficient solid acid catalyst for esterification of oleic acid

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• 作者：Mingbo Wu ; Yang Wang ; Ding Wang ; Minghui Tan ; Peng Li…
• 关键词：Petroleum coke ; Porous carbon ; Solid acid catalyst ; Biodiesel
• 刊名：Journal of Porous Materials
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：23
• 期：1
• 页码：263-271
• 全文大小：1,284 KB
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• 作者单位：Mingbo Wu (1)
  Yang Wang (1)
  Ding Wang (2)
  Minghui Tan (1) (3)
  Peng Li (1)
  Wenting Wu (1)
  Noritatsu Tsubaki (3)
  
  1. State Key Laboratory of Heavy Oil Processing, China University of Petroleum, Qingdao, 266580, China
  2. College of Materials Science and Engineering, University of Shanghai for Science and Technology, Shanghai, 200093, China
  3. Department of Applied Chemistry, Graduate School of Engineering, University of Toyama, Gofuku 3190, Toyama, 930-8555, Japan
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Characterization and Evaluation Materials
  Physical Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1573-4854

文摘

A carbon-based solid acid catalyst was simply prepared from petroleum coke by chemical activation and subsequent sulfonation. The structure–function relationships of the solid acid catalyst were investigated by regulating activation temperature. The materials were characterized by nitrogen adsorption, SEM, XRD, FT-IR and element analysis. The catalytic performances of catalysts were evaluated by the esterification of oleic acid with methanol, which is a crucial reaction in the production of biodiesel. The solid acid catalyst activated at 800 °C exhibits the most excellent catalytic activity, which is attributed to its large surface area (851 m2/g) and high acid density (1.04 mmol/g). At the optimized conditions, high conversion (89.5 %) was achieved and no distinct activity drop was observed after five recycles. This work may offer a facile strategy to fabricate solid acid catalysts in large scale for green chemical processes. Keywords Petroleum coke Porous carbon Solid acid catalyst Biodiesel