Cu(II) and Ni(II) complexes of ferrocene-containing unsaturated β-diketones: electrochemical and burning-rate catalytic properties

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• 作者：Haiying Zhao ; Mingyue Chen ; Xueyou Zhu ; Shufeng Chen…
• 关键词：Ferrocene ; containing unsaturated β ; diketone ; Transition ; metal complex ; Electrochemical property ; Burning ; rate catalyst
• 刊名：Research on Chemical Intermediates
• 出版年：2015
• 出版时间：June 2015
• 年：2015
• 卷：41
• 期：6
• 页码：3971-3980
• 全文大小：624 KB
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• 作者单位：Haiying Zhao (1)
  Mingyue Chen (1)
  Xueyou Zhu (1)
  Shufeng Chen (1)
  Zhanxi Bian (1)
  
  1. College of Chemistry and Chemical Engineering, Inner Mongolia University, Huhhot, 010021, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Physical Chemistry
  Inorganic Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1568-5675

文摘

Ferrocene-containing unsaturated β-diketones and their Cu(II) and Ni(II) complexes have been synthesized and characterized. Cyclic voltammetry investigations revealed that the electron density of the ferrocenyl moieties was influenced by the coordination, making the complexes easier to oxidize than the respective free ligands. Differential thermal analysis (DTA) and thermogravimetry (TG) measurements confirmed the obvious catalytic effect of the Cu(II) and Ni(II) complexes of (1E,6E)-1,7-diferrocenyl-1,6-heptadien-3,5-dione in decreasing the decomposition temperature of ammonium perchlorate (by 68.7 and 41.5?°C, respectively). The results confirm the Cu(II) and Ni(II) complexes of ferrocene-containing unsaturated β-diketones as a kind of potential high-burning-rate catalyst.