Non-isothermal crystallization kinetics and activation energy of bio-based poly(trimethylene terephthalate)/poly(butylene adipate-co-terephthalate) polyester blend

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• 作者：Suresh Dhandapani ; S. K. Nayak ; Smita Mohanty
• 刊名：Polymer Science Series A
• 出版年：2015
• 出版时间：September 2015
• 年：2015
• 卷：57
• 期：5
• 页码：628-634
• 全文大小：823 KB
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• 作者单位：Suresh Dhandapani (1)
  S. K. Nayak (1)
  Smita Mohanty (2)
  
  1. Advanced Research School for Technology and Product Simulation, Central Institute of Plastics Engineering and Technology, Tamil Nadu, Chennai, 600032, India
  2. Laboratory for Advanced Research in Polymeric Materials, Central Institute of Plastics Engineering and Technology, Odisha, Bhubaneswar, 751024, India
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Polymer Sciences
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1555-6107

文摘

The blend of bio-based poly(trimethylene terephthalate)/poly(butylene adipate-co-terephthalate) blend (60/40 by weight ratio) was prepared via melt blending technique using twin screw extrusion. Its non-isothermal crystallization kinetics was investigated by differential scanning calorimetry at different cooling rate. Avrami and Ozawa model was utilized to investigate the crystal growth rate of the blend. The threedimensional crystal growth of the blend was changed into a two-dimensional one with increase of the cooling rate. The blend was crystallized in the form of non-banded spherulites with smaller crystal size. The crystallization activation energy of poly(trimethylene terephthalate) was reduced with the incorporation of poly(butylene adipate-co-terephthalate). The article is published in the original.