Ni(OH)2/MoS x nanocomposite electrodeposited on a flexible CNT/PI membrane as an electrochemical glucose sensor: the synergistic effect of Ni(OH)
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- 作者：Qin Wang ; Yan Zhang ; Weichun Ye ; Chunming Wang
- 关键词：CNT/PI membrane ; Ni(OH)2 nanoparticles ; Molybdenum sulfide ; Nonenzymatic glucose sensor ; Electrocatalytic oxidation
- 刊名：Journal of Solid State Electrochemistry
- 出版年：2016
- 出版时间：January 2016
- 年：2016
- 卷：20
- 期：1
- 页码：133-142
- 全文大小：4,945 KB
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Yan Zhang (1)
Weichun Ye (1)
Chunming Wang (1)
1. College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou, 730000, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Physical Chemistry
Analytical Chemistry
Industrial Chemistry and Chemical Engineering
Characterization and Evaluation Materials
Condensed Matter
Electronic and Computer Engineering - 出版者：Springer Berlin / Heidelberg
- ISSN：1433-0768
文摘
A nonenzymatic glucose sensor was constructed by electrodepositing molybdenum sulfide (MoS x )-nickel (II) hydroxide (Ni(OH)2) in sequence on a flexible carbon nanotube/polyimide (CNT/PI) composite membrane. The sensing material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray powder diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The electrocatalytic activity of the as-prepared nanomaterial toward glucose oxidation was investigated by cyclic voltammetry and amperometric measurement. The Ni(OH)2/MoS x /CNT/PI sensor demonstrated excellent properties including a wide linear range from 10 to 1600 μM of glucose, rapid response (<3 s), low detection limit of 5.4 μM, good selectivity, good repeatability, and long-term stability (2 weeks). The superior performances were attributed to the pronounced synergistic effect between Ni(OH)2 and MoS x . Furthermore, the excellent sensor was successfully applied to detect glucose in human blood serum samples by standard addition method with satisfactory recovery.