Preparation of biodegradable poly(butylene succinate)/halloysite nanotube nanocomposite foams using supercritical CO2 as blowing agent

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• 作者：Wei Wu ; Xianwu Cao ; Hong Lin ; Guangjian He ; Mengmeng Wang
• 关键词：Poly(butylene succinate) ; Halloysite nanotube ; Nanocomposites ; Foam ; Supercritical carbon dioxide
• 刊名：Journal of Polymer Research
• 出版年：2015
• 出版时间：September 2015
• 年：2015
• 卷：22
• 期：9
• 全文大小：3,043 KB
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• 作者单位：Wei Wu (1)
  Xianwu Cao (1)
  Hong Lin (1)
  Guangjian He (1)
  Mengmeng Wang (1)
  
  1. National Engineering Research Center of Novel Equipment for Polymer Processing, Key Laboratory of Polymer Processing Engineering of Ministry of Education, School of Mechanical and Automative Engineering, South China University of Technology, Guangzhou, 510640, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Polymer Sciences
  Industrial Chemistry and Chemical Engineering
  Characterization and Evaluation Materials
  
• 出版者：Springer Netherlands
• ISSN：1572-8935

文摘

Biodegradable poly(butylene succinate) (PBS) was melt compounded with halloysite nanotube (HNT) to prepare PBS/HNT nanocomposites, and both pure PBS and PBS/HNT nanocomposites were foamed successfully using supercritical carbon dioxide as a physical blowing agent. The cell morphologiesshowed that the cell size decreased, and both cell density and volume expansion ratio increased with the addition of HNT. Within the HNT content used in this work (1, 3, 5, and 7?wt.%), the content of 5?wt.% was found to be the one that lead to the smallest cell size and highest cell density and volume expansion ratio. In addition to the HNT content, both saturation temperature and saturation pressure were found to significantly influence the cell morphology. Higher saturation pressure led to smaller cell size and higher volume expansion ratio. Interestingly, a close-celled to interconnect open-celled morphology transition occurred for PBS/HNT nanocomposites at a saturation temperature of 120?°C. The formation of interconnect open-celled morphology was mainly attributed to the stress induced by the HNT in the cell solidification process. With the increase of HNT content, saturation temperature and saturation pressure, the enthalpy of fusion of the foamed samples increased.