Nonenzymatic sensor for glucose based on a glassy carbon electrode modified with Ni(OH)2 nanoparticles grown on a film of molybdenum sulfide
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- 作者：Shanshan Ji ; Zhe Yang ; Chao Zhang ; Yue-E Miao ; Weng Weei Tjiu…
- 关键词：Nonenzymatic glucose sensor ; Electrocatalytic oxidation ; Ni(OH)2 nanoparticles ; Molybdenum sulfide
- 刊名：Microchimica Acta
- 出版年：2013
- 出版时间：August 2013
- 年：2013
- 卷：180
- 期：11-12
- 页码：1127-1134
- 全文大小：1681KB
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Zhe Yang (1)
Chao Zhang (1)
Yue-E Miao (1)
Weng Weei Tjiu (2)
Jisheng Pan (2)
Tianxi Liu (1)
1. State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Fudan University, Shanghai, 200433, China
2. Institute of Materials Research and Engineering, A*STAR (Agency for Science, Technology and Research), 3 Research Link, Singapore, 117602, Singapore - ISSN：1436-5073
文摘
A glassy carbon electrode (GCE) was modified with nickel(II) hydroxide nanoparticles and a film of molybdenum sulfide. The nanocomposite was prepared by two-step electrodeposition. Scanning electron microscopy reveals that the nanoparticles are uniformly deposited on the film. Cyclic voltammetry and chronoamperometry indicate that this modified GCE displays a remarkable electrocatalytic activity towards nonenzymatic oxidation of glucose. Response is linear in the 10-,300 μM concentration range (R 2 --.9987), the detection limit is very low (5.8?μM), response is rapid (< 2?s), and selectivity over ascorbic acid, dopamine, uric acid, fructose and galactose is very good. Figure An efficient nonenzymatic glucose sensor based on Ni(OH)2/MoSx nanocomposite modified glassy carbon electrode has been fabricated via a two-step electrodeposition approach. The resulting nonenzymatic sensor exhibits excellent properties toward glucose detection, such as low detection limit, fast response and noticeable selectivity.