Synthesis of 3-nitramino-4-(1H-1,2,3-triazol-1-yl)-1,2,5-oxadiazoles and their salts

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• 作者：V. Yu. Rozhkov (1) mnn@ioc.ac.ru
  L. V. Batog (1)
  M. I. Struchkova (1)
• 关键词：Key words amino(1 ; 2 ; 3 ; triazol ; 1 ; yl)furazans – ; nitramino(1 ; 2 ; 3 ; triazol ; 1 ; yl)furazans – ; 4 ; amino ; 3 ; azidofurazan – ; 1 ; 3 ; dicarbonyl compounds – ; 1 ; 3 ; cycloaddition – ; nitration – ; hydrolysis – ; decarboxylation – ; nitramino(triazolyl)furazan salts – ; NMR spectroscopy
• 刊名：Russian Chemical Bulletin
• 出版年：2011
• 出版时间：August 2011
• 年：2011
• 卷：60
• 期：8
• 页码：1712-1718
• 全文大小：219.9 KB
• 参考文献：1. L. V. Batog, L. S. Konstantinova, V. Yu. Rozhkov, Yu. A. Strelenko, O. V. Lebedev, L. I. Khmelnitskii, Khim. Geterotsikl. Soedin., 2000, 100 [Chem. Heterocycl. Compd. (Engl. Transl.), 2000, 36, 91].
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• 作者单位：1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991 Moscow, Russian Federation
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Chemistry
  Organic Chemistry
  Inorganic Chemistry
  Russian Library of Science
  
• 出版者：Springer New York
• ISSN：1573-9171

文摘

Nitration of 3-amino-4-(1H-1,2,3-triazol-1-yl)-1,2,5-oxadiazoles (3-amino-4-triazolylfurazans) with a mixture of NaNO₃ and conc. H₂SO₄ gave for the first time triazolylfurazans with a primary nitramino group attached to the furazan ring. If the starting amino(triazolyl)-furazan contains an aromatic substituent, the latter also undergoes nitration under the conditions studied. Some of these nitramines were converted into salts (K, Na, and NH₄).