Exfoliation of graphite by dry ball milling with cellulose
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- 作者：Peipei Sun (1) (2)
Shigenori Kuga (1)
Min Wu (1)
Yong Huang (1) - 关键词：Cellulose ; Graphite ; Ball milling ; Exfoliation ; Electric conductivity
- 刊名：Cellulose
- 出版年：2014
- 出版时间：August 2014
- 年：2014
- 卷：21
- 期：4
- 页码：2469-2478
- 全文大小：3,298 KB
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Shigenori Kuga (1)
Min Wu (1)
Yong Huang (1)
1. Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, 29 Zhongguancun East Road, Haidian District, Beijing, 100190, People’s Republic of China
2. University of Chinese Academy of Sciences, Beijing, 100039, People’s Republic of China - ISSN：1572-882X
文摘
Dry ball milling of graphite with cellulose and related polysaccharides was found effective for exfoliation-dispersion of graphene-like carbon. The exfoliation behavior was found to depend strongly on the polymer species; namely, polysaccharides are much more effective than thermoplastic polymers. The compression-molded slabs from co-milled powder with cellulose and carboxymethylcellulose showed an electrical percolation threshold of 1.0?% (w/w) or lower. The carbon fraction isolated from milling with carboxymethylcellulose was water-dispersible, containing single- to few-layer graphenes. This method can provide facile and solventless graphene exfoliation and mechanical alloying with polymers.