Frequency and Temperature Dependence of Dielectric and Electrical Properties of Sn-Doped Lead Calcium Iron Niobate
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- 作者：Maalti Puri ; Shalini Bahel ; Sukhleen Bindra Narang
- 关键词：Relative permittivity ; loss tangent ; temperature coefficient of relative permittivity ; impedance ; modulus ; activation energy
- 刊名：Journal of Electronic Materials
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：45
- 期：2
- 页码：959-969
- 全文大小：2,783 KB
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Shalini Bahel (1)
Sukhleen Bindra Narang (1)
1. Department of Electronics Technology, Guru Nanak Dev University, Amritsar, Punjab, 143005, India - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Optical and Electronic Materials
Characterization and Evaluation Materials
Electronics, Microelectronics and Instrumentation
Solid State Physics and Spectroscopy - 出版者：Springer Boston
- ISSN：1543-186X
文摘
Sn-substituted lead calcium iron niobate specimens with general formula (Pb0.45Ca0.55)(Fe0.5Nb0.5)1−y Sn y O3 with 0.00 ≤ y ≤ 0.15 in steps of 0.03 have been synthesized using a two-stage method. The x-ray diffraction patterns for all the synthesized samples reveal a perovskite structure with pseudocubic symmetry. A small amount of pyrochlore phase was obtained along with the perovskite phase, decreasing with increasing Sn content up to y = 0.09. The temperature and frequency dependence of the dielectric and electrical properties of Sn-substituted lead calcium iron niobate were studied. Two dielectric anomalies were observed in ε r–T plots for all the samples due to generation of oxygen vacancies. The temperature coefficient of relative permittivity, τ ε , decreased with increasing Sn content. The single, semicircular arc observed in Nyquist plots suggests a single relaxation process. The activation energies obtained from the temperature dependence of the relaxation time and grain resistance were found to be approximately comparable. Keywords Relative permittivity loss tangent temperature coefficient of relative permittivity impedance modulus activation energy