Induced crystallization behavior of poly(ethylene adipate) by highly oriented polyethylene

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• 作者：Chun-zhu Yan (11292)
  Lin Guo (11292)
  Hai-bo Chang (21292)
  Shou-ke Yan (31292)
  
• 关键词：Poly(ethylene adipate) ; Polyethylene ; Epitaxy ; Orientation
• 刊名：Chinese Journal of Polymer Science
• 出版年：2013
• 出版时间：August 2013
• 年：2013
• 卷：31
• 期：8
• 页码：1173-1182
• 全文大小：853KB
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• 作者单位：Chun-zhu Yan (11292)
  Lin Guo (11292)
  Hai-bo Chang (21292)
  Shou-ke Yan (31292)
  
  11292. School of Chemistry and Environment, Beihang University, Beijing, 100191, China
  21292. Chemistry and Chemical Engineering College, Henan University, Kaifeng, 475001, China
  31292. State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, China
  

文摘

The crystallization behavior of poly(ethylene adipate) (PEA) on highly oriented high-density polyethylene (PE) substrate both from solution and isotropic melt was studied by means of optical microscopy, differential scanning calorimetry, atomic force microscopy and electron diffraction. The results show that the PE influences the crystallization of PEA strongly, which results in an epitaxial growth of PEA with well ordered structure. At the boundary of the PE substrate, a transcrystalline PEA layer is observed. Fine structural observation illustrates that the PEA grows on the PE substrate in edgeon lamellae with fixed orientation. Electron diffraction demonstrates that the epitaxial organization of PEA on PE occurs with both polymer chains parallel, which leads to the (00l) PEA diffractions inclined ±23.5° to the chain direction of PE crystals. Combining the real space morphological observation and electron diffraction results, it is concluded that the epitaxial PEA edge-on lamellae are folded in the {00l} lattice planes.