Molecular imaging of paper cross sections by FT-IR spectroscopy and principal component analysis

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• 作者：S. Genest (1) (2)
  R. Salzer (3)
  G. Steiner (4)
  
• 关键词：Fourier transform infrared imaging ; Paper cross section ; Wet strength ; Poly(amidoamine)–epichlorohydrin
• 刊名：Analytical and Bioanalytical Chemistry
• 出版年：2013
• 出版时间：June 2013
• 年：2013
• 卷：405
• 期：16
• 页码：5421-5430
• 全文大小：521KB
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• 作者单位：S. Genest (1) (2)
  R. Salzer (3)
  G. Steiner (4)
  
  1. Leibniz-Institut für Polymerforschung Dresden e.V., P.O. Box 120 411, 01005, Dresden, Germany
  2. Organische Chemie der Polymere, Technische Universit?t Dresden, 01062, Dresden, Germany
  3. Department of Chemistry and Food Chemistry, Dresden University of Technology, 01062, Dresden, Germany
  4. Clinical Sensoring and Monitoring, Faculty of Medicine, Dresden University of Technology, Fetscher Str. 74, 01307, Dresden, Germany
  
• ISSN：1618-2650

文摘

The molecular imaging of paper cross sections containing the wet-strength additive poly(amidoamine)–epichlorohydrin (PAE) was effected by Fourier transform infrared (FT-IR) spectroscopic imaging. Thin cross sections of laboratory sheet samples were prepared and transferred onto CaF2ub> substrates. A laboratory sheet sample without PAE acted as a reference. Principal component analysis (PCA) was applied to identify and to reveal the distribution of PAE across the section. Differences in the loading plots of the fourth and fifth principal components for the sheets with and without PAE were found in the region of the amide I, amide II, and amine bands within a variance of 0.4-.8?%. The score images of the PCA reveal inhomogeneous distribution of PAE. Small areas of higher concentration of PAE occur across the cross section. The aim of this study was to demonstrate that FT-IR spectroscopic imaging provides spatially resolved quantitative information about the chemical composition of paper, which was successfully achieved. Figure New analytical approach for imaging paper cross sections at molecular level