H3PW12O40 supported on mesoporous MCM-41 and Al–MCM-41 materials: preparation and characterisation
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- 作者：1. Institute of Biodiversity and Ecosystems Research ; Bulgarian Academy of Sciences ; Sofia ; Bulgaria2. Dipartimento di Chimica “S. Cannizzaro- Università di Palermo and INSTM-Udr Palermo ; Parco d’Orleans II Viale delle Scienze pad 17 ; 90128 Palermo ; Italy3. Centro Grandi Apparecchiature—UniNetLab ; Università di Palermo ; Via F. Marini 14 ; 90128 Palermo ; Italy
- 刊名：Journal of Materials Science
- 出版年：2011
- 出版时间：November 2011
- 年：2011
- 卷：46
- 期：22
- 页码：7114-7120
- 全文大小：431.7 KB
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- 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Materials Science
Characterization and Evaluation Materials
Polymer Sciences
Continuum Mechanics and Mechanics of Materials
Crystallography
Mechanics - 出版者：Springer Netherlands
- ISSN：1573-4803
文摘
MCM-41 and Al–MCM-41 has been synthesized using cetyl-trimethylammonium bromide (CTAB) surfactant as template and adding the silica precursor to aqueous solutions containing CTAB. The obtained solids were calcined at 600 °C for 4 h. HPW heteropolyacid supported on the mesoporous were prepared using the incipient wetness method. The characterization of materials was performed by X-ray diffraction, Transmission Electron Microscopy, N2 adsorption, 29Si Cross Polarization–Magic Angle Spinning and 27Al MAS NMR. Results showed that the hexagonal structure is obtained in both cases. The Aluminium species are located inside an extra-framework. The impregnation reduces the surface area of the mesoporous materials especially of the Al–MCM-41 suggesting a participation of aluminium during the impregnation. HPW is well dispersed in the mesoporous materials and is located inside the pores interacting with the silanol group of the pores wall. 27Al MAS NMR measurements have showed that the impregnation causes the removal of the non-framework aluminium.