Simultaneous Determination of Indole-3-Acetic Acid and Indole-3-Butyric Acid in Plant by Field-Amplified Sample Stacking Open-Tubular Capillary Electrochromatography Based on Solid-Phase Extraction with Calixarene Sorbent
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- 作者：Liu Yang ; Yanlong Chen ; Shengnan Zhao ; Wenfen Zhang ; Huifang Du…
- 关键词：Indole ; 3 ; acetic acid ; Beta ; indolebutyric acid ; Open ; tubular capillary electrochromatography ; Methyldiethanolamine amination polychloromethyl styrene ; SPE
- 刊名：Chromatographia
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：79
- 期：3-4
- 页码：243-254
- 全文大小：1,268 KB
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Yanlong Chen (1)
Shengnan Zhao (1)
Wenfen Zhang (1)
Huifang Du (1)
Zhifen Deng (1)
Shusheng Zhang (1)
1. College of Chemistry and Molecular Engineering, Zhengzhou University, Kexue Rd 100, Zhengzhou, 450001, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Analytical Chemistry
Organic Chemistry
Pharmacy
Biochemistry
Plant Sciences
Measurement Science and Instrumentation - 出版者：Vieweg Verlag
- ISSN：1612-1112
文摘
This paper describes the preparation and application of methyldiethanolamine amination polychloromethyl styrene nanolatex (MDEAPL) and MDEAPL coated capillary column (ccc-MDEAPL). The ccc-MDEAPL column was characterized with steady EOF values from −14.6 × 10−5 to −19.8 × 10−5 at pH 7.08–7.56. A method using tetraazacalix[2]arene[2]triazine-modified silica gel (NCS) as solid-phase extraction (SPE) sorbent was developed for concentrating and purifying the two phytohormones, indole-3-acetic acid (IAA) and beta-indolebutyric acid (IBA) of different plants. The determination conditions of IAA and IBA for field-amplified sample stacking open-tubular capillary electrochromatography based on SPE with NCS sorbent (NCS-SPE-FASS-OT-CEC) were optimized as follows: background electrolyte, 30 mmol L−1 Tris + 24 mmol L−1 HClO4 (30 % acetonitrile, pH 7.24); ccc-MDEAPL, 50 μm i.d. × 50 cm (effective length 41.5 cm); separation voltage, −25 kV; column temperature, 25 °C; UV detection wavelength, 230 nm; water-plug injection, 30 mbar × 20 s; sample electrokinetic injection, −20 kV × 20 s. Under the optimized conditions, IAA and IBA were well separated within 6 min (Rs > 1.5). The NCS-SPE-FASS-OT-CEC method was validated in terms of linearity, sensitivity, selectivity, precision and accuracy. The detection limits were 8 ng mL−1 for IAA and 25 ng mL−1 for IBA (S/N = 3), respectively. The overall recoveries ranged from 81.0 to 89.0 %. The developed method was successfully applied for the determination of IAA and IBA in different positions of various plants. Keywords Indole-3-acetic acid Beta-indolebutyric acid Open-tubular capillary electrochromatography Methyldiethanolamine amination polychloromethyl styrene SPE