Novel molybdenum complexes with the 3,6-Di-tert-butylcatecholate ligand
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- 作者：P. A. Petrov ; M. Yu. Afonin ; D. Yu. Naumov…
- 刊名：Russian Journal of Coordination Chemistry
- 出版年：2015
- 出版时间：January 2015
- 年：2015
- 卷：41
- 期：1
- 页码：31-36
- 全文大小：355 KB
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- 刊物主题：Chemistry
Physical Chemistry
Inorganic Chemistry
Russian Library of Science - 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
- ISSN：1608-3318
文摘
A reaction of the cluster (Et4N)2[Mo3S7Br6] with potassium 3,6-di-tert-butyl-o-benzosemiquinolate (KSQ36) afforded the mononuclear complexes (Et4N)[Mo(Cat36)3] (I) and (Et4N)[MoO(Cat36)2(HCat36)] (II) with prismatic and octahedral environments of their central metal atoms, respectively. Complex I was also obtained by a reaction between MoCl5, sodium 3,6-di-tert-butylcatecholate (Na2Cat36), and Et4NBr. Complexes I and II were characterized by X-ray diffraction and EPR spectroscopy. The structures have been deposited with the Cambridge Structural Database (nos. 1009139 (I), 1009140 (I · 1.5THF), and 1009141 (II · Et2O)).