Analysis of Parent/Nitrated Polycyclic Aromatic Hydrocarbons in Particulate Matter 2.5 Based on Femtosecond Ionization Mass Spectrometry

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• 作者：Noboru Itouyama ; Taiki Matsui…
• 关键词：Gas chromatography ; Multiphoton ionization ; Time ; of ; flight mass spectrometry ; Particulate matter 2.5 ; Polycyclic aromatic hydrocarbons ; Nitrated polycyclic aromatic hydrocarbons
• 刊名：Journal of The American Society for Mass Spectrometry
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：27
• 期：2
• 页码：293-300
• 全文大小：817 KB
• 参考文献：1.Miller, F.J., Gardner, D.E., Graham, J.A., Lee Jr., R.E., Wilson, W.E., Bachmann, J.D.: Size considerations for establishing a standard for inhalable particles. J. Air Poll. Control Assoc. 29, 610–615 (1979)CrossRef
  2.Denissenko, M.F., Pao, A., Tang, M., Pfeifer, G.P.: Preferential formation of benzo[a]pyrene adducts at lung cancer mutational hotspots in P53. Science 274, 430–432 (1996)CrossRef
  3.Manzano, C., Hoh, E., Simonich, S.L.M.: Quantification of complex polycyclic aromatic hydrocarbon mixtures in standard reference materials using comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry. J. Chromatogr. A 1307, 172–179 (2013)CrossRef
  4.Hung, C.-H., Ho, H.-P., Lin, M.-T., Chen, C.-Y., Shu, Y.-Y., Lee, M.-R.: Purge-assisted headspace solid-phase microextraction combined with gas chromatography/mass spectrometry for the determination of trace nitrated polycyclic aromatic hydrocarbons in aqueous samples. J. Chromatogr. A 1265, 1–6 (2012)CrossRef
  5.Fendt, A., Geissler, R., Streibel, T., Sklorz, M., Zimmermann, R.: Hyphenation of two simultaneously employed soft photo ionization mass spectrometers with thermal analysis of biomass and biochar. Thermochim. Acta 551, 155–163 (2013)CrossRef
  6.Minomo, K., Ohtsuka, N., Nojiri, K., Hosono, S., Kawamura, K.: A simplified determination method of dioxin toxic equivalent (TEQ) by single GC/MS measurement of five indicative congeners. Anal. Sci. 27, 421–426 (2011)CrossRef
  7.Weggler, B.A., Gröger, T., Zimmermann, R.: Advanced scripting for the automated profiling of two-dimensional gas chromatography-time-of-flight mass spectrometry data from combustion aerosol. J. Chromatogr. A 1364, 241–248 (2014)CrossRef
  8.Lopes, W.A., da Rocha, G.O., de P. Pereira, P.A., Oliveira, F.S., Carvalho, L.S., de C. Bahia, N., dos S. Conceição, L., de Andrade, J.B.: Multivariate optimization of a GC-MS method for determination of sixteen priority polycyclic aromatic hydrocarbons in environmental samples. J. Sep. Sci. 31, 1787–1796 (2008)
  9.Imasaka, T.: Gas chromatography/multiphoton ionization/time-of-flight mass spectrometry using a femtosecond lase. Anal. Bioanal. Chem. 405, 6907–6912 (2013)CrossRef
  10.Shitamichi, O., Matsui, T., Hui, Y., Chen, W., Imasaka, T.: Determination of persistent organic pollutants by gas chromatography/laser multiphoton ionization/time-of-flight mass spectrometry. Front. Environ. Sci. Eng. 6, 26–31 (2012)CrossRef
  11.Bente, M., Adam, T., Ferge, T., Gallavardin, S., Sklorz, M., Streibel, T., Zimmermann, R.: An on-line aerosol laser mass spectrometer with three, easily interchangeable laser based ionisation methods for characterization of inorganic and aromatic compounds on particles. Int. J. Mass Spectrom. 258, 86–94 (2006)CrossRef
  12.Sakurai, S., Uchimura, T.: Pyrolysis-gas chromatography/multiphoton ionization/time-of-flight mass spectrometry for the rapid and selective analysis of polycyclic aromatic hydrocarbons in aerosol particulate matter. Anal. Sci. 30, 891–895 (2014)CrossRef
  13.Albinet, A., Leoz-Garziandia, E., Budzinski, H., Villenave, E.: Simultaneous analysis of oxygenated and nitrated polycyclic aromatic hydrocarbons on standard reference material 1649a (urban dust) and on natural ambient air samples by gas chromatography–mass spectrometry with negative ion chemical ionization. J. Chromatogr. A 1121, 106–113 (2006)CrossRef
  14.Masiol, M., Centanni, E., Squizzato, S., Hofer, A., Pecorari, E., Rampazzo, G., Pavoni, B.: GC-MS analyses and chemometric processing to discriminate the local and long-distance sources of PAHs associated to atmospheric PM2.5. Environ. Sci. Pollut. Res. 19, 3142–3151 (2012)CrossRef
  15.Tsuji, N., Matsuzaki, Y., Hayashi, S.: Real-time detection of 1-nitronaphthalene in atmosphere by single-photon ionization mass spectrometry. Bunseki Kagaku 61, 359–365 (2012)CrossRef
  16.Hamachi, A., Okuno, T., Imasaka, T., Kida, Y., Imasaka, T.: Resonant and nonresonant multiphoton ionization processes in the mass spectrometry of explosives. Anal. Chem. 87, 3027–3031 (2015)CrossRef
  17.Matsumoto, J., Saito, G., Imasaka, T.: Use of ring-repeller, double-skimmer electrodes for efficient ion focusing in mass spectrometry. Anal. Sci. 18, 567–570 (2002)CrossRef
  18.Matsumoto, J., Nakano, B., Imasaka, T.: Development of a compact supersonic jet/multiphoton ionization/time-of-flight mass spectrometer for the on-site analysis of dioxin. Part I. Evaluation of basic performance. Anal. Sci. 19, 379–382 (2003)CrossRef
  19.Matsumoto, J., Nakano, B., Imasaka, T.: Development of a compact supersonic jet/multiphoton ionization/time-of-flight mass spectrometer for the on-site analysis of dioxin. Part II. Application to chlorobenzene and dibenzofuran. Anal. Sci. 19, 383–386 (2003)CrossRef
  20.Kawanaka, Y., Sakamoto, K., Wang, N., Yun, S.-J.: Simple and sensitive method for determination of nitrated polycyclic aromatic hydrocarbons in diesel exhaust particles by gas chromatography-negative ion chemical ionization tandem mass spectrometry. J. Chromatogr. A 1163, 312–317 (2007)CrossRef
  21.Manual on Determination of Dioxins in Ambient Air, the Ministry of Environment, Japan. Available at: https://​www.​env.​go.​jp/​en/​chemi/​dioxins/​manual.​pdf . Accessed 26 Sept 2015
  22.Yan, J., Wang, L., Fu, P.P., Yu, H.: Photomutagenicity of 16 polycyclic aromatic hydrocarbons from the US EPA priority pollutant list. Mutat. Res. 557, 99–108 (2004)CrossRef
  23.Asare, N., Landvik, N.E., Lagadic-Gossmann, D., Rissel, M., Tekpil, X., Ask, K., Lag, M., Holme, J.A.: 1-Nitropyrene (1-NP) induces apoptosis and apparently a non-apoptotic programmed cell death (paraptosis) in Hepa1c1c7 cells. Toxicol. Appl. Pharmacol. 230, 175–186 (2008)CrossRef
  24.Zhang, Y.-L., Huang, R.-J., El Haddar, I., Ho, K.-F., Cao, J.-J., Han, Y., Zotter, P., Bozzetti, C., Daellenbach, K.R., Canonaco, F., Slowik, J.G., Salazar, G., Schwikowski, M., Schnelle-Kreis, J., Abbaszade, G., Zimmermann, R., Baltensperger, U., Prévôt, A.S.H., Szidat, S.: Fossil versus non-fossil sources of fine carbonaceous aerosols in four Chinese cities during the extreme winter haze episode of 2013. Atmos. Chem. Phys. 15, 1299–1312 (2015)CrossRef
  25.Imasaka, T., Imasaka, T.: An evaluation of the spectral properties of nerve agents for laser ionization mass spectrometry. Anal. Sci. 30, 1113–1120 (2014)CrossRef
  26.Tang, Y., Imasaka, T., Yamamoto, S., Imasaka, T.: Multiphoton ionization mass spectrometry of nitrated polycyclic aromatic hydrocarbons. Talanta 140, 109–114 (2015)CrossRef
  27.Frisch, M.J., Trucks, G.W., Schlegel, H.B., Scuseria, G.E., Robb, M.A., Cheeseman, J.R., Scalmani, G., Barone, V., Mennucci, B., Petersson, G.A., Nakatsuji, H., Caricato, M., Li, X., Hratchian, H.P., Izmaylov, A.F., Bloino, J., Zheng, G., Sonnenberg, J.L., Hada, M., Ehara, M., Toyota, K., Fukuda, R., Hasegawa, J., Ishida, M., Nakajima, T., Honda, Y., Kitao, O., Nakai, H., Vreven, T., Montgomery, J.A., Jr., Peralta, J.E., Ogliaro, F., Bearpark, M., Heyd, J.J., Brothers, E., Kudin, K.N., Staroverov, V.N., Kobayashi, R., Normand, J., Raghavachari, K., Rendell, A., Burant, J.C., Iyengar, S.S., Tomasi, J., Cossi, M., Rega, N., Millam, J.M., Klene, M., Knox, J.E., Cross, J.B., Bakken, V., Adamo, C., Jaramillo, J., Gomperts, R., Stratmann, R.E., Yazyev, O., Austin, A.J., Cammi, R., Pomelli, C., Ochterski, J.W., Martin, R.L., Morokuma, K., Zakrzewski, V.G., Voth, G.A., Salvador, P., Dannenberg, J.J., Dapprich, S., Daniels, A.D., Farkas, Ö., Foresman, J.B., Ortiz, J.V., Cioslowski, J., Fox, D.J.: Gaussian 09, Revision D.01: Gaussian, Inc., Wallingford CT (2009)
  28.Matsui, T., Fukazawa, K., Fujimoto, M., Imasaka, T.: Analysis of persistent organic pollutants at sub-femtogram levels using a high-power picosecond laser for multiphoton ionization in conjunction with gas chromatography/time-of-flight mass spectrometry. Anal. Sci. 28, 445–450 (2012)CrossRef
  29.Oukebdane, K., Portet-Koltalo, F., Machour, N., Dionnet, F., Desbène, P.L.: Comparison of hot soxhlet and accelerated solvent extractions with microwave and supercritical fluid extractions for the determination of polycyclic aromatic hydrocarbons and nitrated derivatives strongly adsorbed on soot collected inside a diesel particulate filter. Talanta 82, 227–236 (2010)CrossRef
  30.Richter, H., Howard, J.B.: Formation of polycyclic aromatic hydrocarbons and their growth to soot—a review of chemical reaction pathways. Prog. Energy Combust. Sci. 26, 565–608 (2000)CrossRef
  31.Bockhorn, H.: Soot formation in combustion: mechanisms and models; Springer Series in Chemical Physics (1st ed. Vol. 59): Berlin (1994)
  32.Di Filippo, P., Riccardi, C., Pomata, D., Buiarelli, F.: Concentrations of PAHs, and nitro- and methyl-derivatives associated with a size-segregated urban aerosol. Atmos. Environ. 44, 2742–2749 (2010)CrossRef
  33.Hayakawa, K., Murahashi, T., Butoh, M., Miyazaki, M.: Determination of 1,3-, 1,6-, and 1,8-dinitropyrenes and 1-nitropyrene in urban air by high-performance liquid chromatography using chemiluminescence detection. Environ. Sci. Technol. 29, 928–932 (1995)CrossRef
  34.Hayashi, R., Kowhakul, W., Susa, A., Koshi, M.: Detection of explosives using a vacuum ultraviolet ionization time-of-flight mass spectrometry (VUV-TOFMS). Sci. Tech. Energ. Mat. 70, 62–67 (2009)
  35.Wang, W., Jariyasopit, N., Schrlau, J., Jia, Y., Tao, S., Yu, T., Dashwood, R.H., Zhang, W., Wang, X., Simonich, S.L.: Concentration and photochemistry of PAHs, NPAHs, and OPAHs and toxicity of PM2.5 during the Beijing Olympic Games. Environ. Sci. Technol. 45, 6887–6895 (2011)CrossRef
  
• 作者单位：Noboru Itouyama (1)
  Taiki Matsui (1)
  Shigekazu Yamamoto (2)
  Tomoko Imasaka (3)
  Totaro Imasaka (1) (4)
  
  1. Department of Applied Chemistry, Graduate School of Engineering, Kyushu University, Nishi-ku, Fukuoka, 819-0395, Japan
  2. Fukuoka Institute of Health and Environmental Sciences, Dazaifu, Fukuoka, 818-0135, Japan
  3. Laboratory of Chemistry, Graduate School of Design, Kyushu University, Minami-ku, Fukuoka, 815-8540, Japan
  4. Division of Optoelectronics and Photonics, Center for Future Chemistry, Kyushu University, Nishi-ku, Fukuoka, 819-0395, Japan
  
• 刊物主题：Analytical Chemistry; Biotechnology; Organic Chemistry; Proteomics; Bioinformatics;
• 出版者：Springer US
• ISSN：1879-1123

文摘

Particulate matter 2.5 (PM2.5), collected from ambient air in Fukuoka City, was analyzed by gas chromatography combined with multiphoton ionization mass spectrometry using an ultraviolet femtosecond laser (267 nm) as the ionization source. Numerous parent polycyclic aromatic hydrocarbons (PPAHs) were observed in a sample extracted from PM2.5, and their concentrations were determined to be in the range from 30 to 190 pg/m3 for heavy PPAHs. Standard samples of nitrated polycyclic aromatic hydrocarbons (NPAHs) were examined, and the limits of detection were determined to be in the picogram range. The concentration of NPAH adsorbed on PM2.5 in the air was less than 900–1300 pg/m3.