Characterization of γ and γ′ phases in 2nd and 4th generation single crystal nickel-base superalloys
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- 作者：Maciej Zietara ; Steffen Neumeier ; Mathias Göken…
- 关键词：superalloy ; NI ; AFM ; nanoindentation ; rafting ; creep
- 刊名：Metals and Materials International
- 出版年：2017
- 出版时间：January 2017
- 年：2017
- 卷：23
- 期：1
- 页码：126-131
- 全文大小：
- 刊物类别：Chemistry and Materials Science
- 刊物主题：Metallic Materials; Operating Procedures, Materials Treatment; Magnetism, Magnetic Materials; Engineering Thermodynamics, Heat and Mass Transfer; Characterization and Evaluation of Materials; Continuu
- 出版者：The Korean Institute of Metals and Materials
- ISSN：2005-4149
- 卷排序：23
文摘
A Ni based single crystal superalloy from the 2nd generation, PWA 1484, and one from the 4th generation, PWA 1497, were comparatively studied by scanning electron microscopy, energy dispersive X-ray spectroscopy and nanoindentation technique in an atomic force microscope (NI-AFM) after high temperature creep deformation. During primary creep of both generations of superalloys, γ′ precipitates start to coalesce and grow directionally. Further creep deformation leads to the topological inversion and coarsening of the rafted microstructure. The NI-AFM technique was used for measurements of the hardness of the γ and γ′ phases in as-received and creep deformed samples in various conditions. The g matrix of the PWA 1497 superalloy is on average 0.8 GPa harder than that of PWA 1484 that can be explained by higher content of Re and Ru, since they partition predominantly to the matrix phase.