Heteronuclear Cu(II)–Mn(II)–Cu(II) Complex Constructed from Metallo-Ligand Through Carboxylate Oxygens: Coexistence of Water Hexamers

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• 作者：Ting Chen (1)
  Yang Zou (1) zouyang@zstu.edu.cn
  Chaoyong Yu (1)
  Xiaojun Zhou (1)
  Yuanyuan Li (1)
• 关键词：Metallo ; ligand – Water cluster – Dipeptide – Hydrogen bond – Self assembly
• 刊名：Journal of Inorganic and Organometallic Polymers and Materials
• 出版年：2012
• 出版时间：September 2012
• 年：2012
• 卷：22
• 期：5
• 页码：1200-1205
• 全文大小：440.3 KB
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• 作者单位：1. Zhejiang Sci-Tech University, Hangzhou, Zhejiang, China
• ISSN：1574-1451

文摘

A heteronuclear complex of [Mn(H₂O)₄(CuL)₂]₂·4H₂O 1 (H₂L = 2-hydrogen benzaldehydeneglycylglycine) has been synthesized and characterized by IR spectra, TGA, and single crystal X-ray diffraction analysis. The molecule consists of one \textMn(\textH₂\textO)₄2+\text{Mn}{(\text{H}_{2}\text{O})_{4}}^{2+} Mn(H₂O)₄2+ group and two symmetric groups [CuL]? which are connected by carboxylate oxygen atoms. A discrete water hexamer composed of a planar tetrameric water ring and two pendent water molecules acts as a ‘glue’ to assemble adjacent [CuL]? into a two-dimensional structure.