Extraction of humic substances from fresh waters on solid-phase cartridges and their study by Fourier transform ion cyclotron resonance mass spectrometry

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• 作者：A. Ya. Zherebker ; I. V. Perminova ; A. I. Konstantinov…
• 关键词：humic substances ; fresh water ; extraction ; solid ; phase cartridge ; XAD ; 8 ; selective adsorption ; Fourier transform mass spectrometry
• 刊名：Journal of Analytical Chemistry
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：71
• 期：4
• 页码：372-378
• 全文大小：650 KB
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• 作者单位：A. Ya. Zherebker (1)
  I. V. Perminova (1)
  A. I. Konstantinov (1)
  A. B. Volikov (1)
  Yu. I. Kostyukevich (2) (3)
  A. S. Kononikhin (2) (3)
  E. N. Nikolaev (2) (3)
  
  1. Department of Chemistry, Moscow State University, Moscow, 119991, Russia
  2. Institute of Biochemical Phyiscs, Russian Academy of Sciences, ul. Kosygina 4, Moscow, 119334, Russia
  3. Institute of Energy Problems for Chemical Physics, Russian Academy of Sciences, Leninskii pr. 38, Moscow, 119334, Russia
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1608-3199

文摘

Humic substances (HS) have been extracted from fresh waters on macroporous adsorbents of different types, Amberlite XAD-8 resin and Bond Elute PPL solid-phase cartridge. Comparative analysis of the extracted samples by ultra-high resolution mass spectrometry demonstrated selectivity of the selected adsorbents to the components of the molecular assembly of HS: the XAD-8 resin has affinity to the higher oxidized aromatic compounds and PPL has affinity to substances of stronger aliphatic character and nitrogen-containing compounds. Because of this fact, a comparison of the molecular composition of HS isolated from various sources must be performed taking into account selective adsorption; therefore, it is necessary to compare the products extracted by the same adsorbent for correct interpretation.