Adhesive bonding between polyamide and steel

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• 作者：V. I. Vettegren-/a> ; A. Ya. Bashkarev ; A. V. Savitskii ; I. P. Shcherbakov…
• 刊名：Technical Physics
• 出版年：2015
• 出版时间：August 2015
• 年：2015
• 卷：60
• 期：8
• 页码：1257-1260
• 全文大小：183 KB
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• 作者单位：V. I. Vettegren-/a> (1)
  A. Ya. Bashkarev (2)
  A. V. Savitskii (1)
  I. P. Shcherbakov (1)
  V. V. Sytov (3)
  R. I. Mamalimov (1)
  
  1. Ioffe Physical Technical Institute, Russian Academy of Sciences, Politekhnicheskaya ul. 26, St. Petersburg, 194021, Russia
  2. St. Petersburg State Polytechnical University, Politekhnicheskaya ul. 29, St. Petersburg, 195251, Russia
  3. Research and Production Company STEP, ul. Kalinina 13, St. Petersburg, 198099, Russia
  
• 刊物类别：Physics and Astronomy
• 刊物主题：Physics
  Mechanics, Fluids and Thermodynamics
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1090-6525

文摘

Fluorescence and IR absorption spectra are taken of coatings obtained by applying polyamide 6 powder on a steel substrate heated above the polymer melting point and subsequently cooling to room temperature. It follows from the coating spectra that the energy of a π* ?n transition in the C—O bonds of polyamide decreases. Simultaneously, the maximum of a band assigned to the deformation vibrations of N—H bonds shifts toward longer wavelengths. These effects are explained by the formation of coordination bonds between Fe2+ ions having diffused from the steel into the polymer and nitrogen atoms entering into polyamide 6 molecules. As a result, a coordination-compound-saturated diffusion layer up to 100 μm thick arises near the steel surface. Coordination compounds squeeze the framework of the polyamide 6 molecule roughly by 0.06%. Eventually, a polyamide layer that is stronger than the surroundings appears at the polyamide 6—steel interface.