Vortex-Assisted Ionic Liquid Dispersive Liquid-Liquid Microextraction Coupled with High-Performance Liquid Chromatography for the Determination of Triazole Fungicides in Fruit Juices
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- 作者：Yaohai Zhang ; Yan Zhang ; Qiyang Zhao ; Weijun Chen ; Bining Jiao
- 关键词：Ionic liquid (IL) ; Dispersive liquid ; liquid microextraction (DLLME) ; High ; performance liquid chromatography (HPLC) ; Triazole fungicides ; Fruit juices
- 刊名：Food Analytical Methods
- 出版年：2016
- 出版时间：March 2016
- 年：2016
- 卷：9
- 期：3
- 页码：596-604
- 全文大小：659 KB
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Yan Zhang (1) (6)
Qiyang Zhao (1) (2) (3)
Weijun Chen (1) (2) (3)
Bining Jiao (1) (2) (3) (4) (5)
1. Citrus Research Institute, Southwest University, Chongqing, 400712, People’s Republic of China
2. Laboratory of Quality and Safety Risk Assessment for Citrus Products, Ministry of Agriculture, Chongqing, 400712, People’s Republic of China
3. Quality Supervision and Testing Centre for Citrus and Seedling, Ministry of Agriculture, Chongqing, 400712, People’s Republic of China
6. College of Horticulture and Landscape Architecture, Southwest University, Chongqing, 400716, People’s Republic of China
4. National Citrus Engineering Research Center, Chongqing, 400712, People’s Republic of China
5. Chongqing Key Laboratory of Citrus Sciences, Chongqing, 400712, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Food Science
Chemistry
Microbiology
Analytical Chemistry - 出版者：Springer New York
- ISSN：1936-976X
文摘
A rapid, efficient, and environmentally friendly method using vortex-assisted ionic liquid dispersive liquid-liquid microextraction (VA-IL-DLLME) prior to high-performance liquid chromatography coupled with photodiode array detection (HPLC-PDA) has been developed for the determination of six triazole fungicides (triazolone, triadimenol, epoxiconazole, flusilazole, tebuconazole, and diniconazole) in various fruit juices. 1-Hexyl-3-methylimidazolium hexafluorophosphate ([C6MIM][PF6]) and acetonitrile were used as extraction and dispersive solvents, respectively. A single factor experiment was selected to obtain the significant variables from the several related parameters that could affect the extraction efficiencies, such as the volume of IL and acetonitrile, extraction time, centrifugation time, and salt addition. Under the optimum conditions, an excellent linearity with correlation coefficients higher than 0.997 was obtained. Enrichment factors and average recoveries in three concentration levels ranged from 51 to 72, and 71.0 to 104.5 %, respectively, and the relative standard deviations (RSDs) from 1.4 to 11.8 %. The limits of detection (LODs) (S/N = 3) for the six triazole fungicides were between 0.4 and 6.7 μg L−1. The proposed method was successfully applied for the determination of trace amounts of triazole fungicides in various fruit juices including peach, apple, and orange juices. Keywords Ionic liquid (IL) Dispersive liquid-liquid microextraction (DLLME) High-performance liquid chromatography (HPLC) Triazole fungicides Fruit juices