Determination of Seven Odorants in Purified Water Among Worldwide Brands by HS-SPME Coupled to GC–MS

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• 作者：Shifu Peng (1)
  Zhen Ding (1) (2)
  Lei Zhao (3)
  Juan Fei (2)
  Zhoubin Xuan (4)
  Chenxi Huang (4)
  Xiaodong Chen (1) (2)
  
• 关键词：HS ; SPME/GC–MS ; Odorants ; Purified water ; Geosmin ; Dimethyl trisulfide
• 刊名：Chromatographia
• 出版年：2014
• 出版时间：May 2014
• 年：2014
• 卷：77
• 期：9-10
• 页码：729-735
• 全文大小：
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• 作者单位：Shifu Peng (1)
  Zhen Ding (1) (2)
  Lei Zhao (3)
  Juan Fei (2)
  Zhoubin Xuan (4)
  Chenxi Huang (4)
  Xiaodong Chen (1) (2)
  
  1. School of Public Health, Southeast University, Nanjing, 210009, China
  2. Department of Environmental and Endemic Diseases Control, Jiangsu Center for Disease Control and Prevention, Nanjing, 210009, China
  3. Clinical School, Southeast University, Nanjing, 210009, China
  4. Department of Environmental Health, Yangpu Center for Disease Control and Prevention, Shanghai, 200090, China
  
• ISSN：1612-1112

文摘

Musty and earthy odors dramatically influence the esthetic quality and consumer acceptability of drinking water. This study was conducted to obtain a sensitive method for simultaneous analysis of seven odors, including geosmin (GSM), 2-methylisoborneol (2-MIB), 2-isopropyl-3-methoxy pyrazine (IPMP), dimethyl trisulfide (DMTS), 2,4,6-trichloroanisole (2,4,6-TCA), β-cyclocitral, and β-ionone, in water by applying headspace solid phase micro-extraction coupled to gas chromatography with mass spectrometry. Moreover, the proposed method was applied to obtain preliminary understanding of the levels of these odorants in purified water among various brands in the world, and to try to find out the potential causes when the odorants appeared in purified water. The target compounds could be separated and analyzed effectively within 23?min, and the GSM and DMTS could be detected in all brands of chosen countries, while the IPMP, β-ionone and 2,4,6-TCA cannot be observed in the above brands.