Metallosupramolecular Silver and Zinc Complexes with Flexible or Semirigid Tripodal Pyridyl Pyrimidine Ligands
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- 作者：Huaze Dong ; Xia Liu ; Bin Zheng ; Yanping Wang…
- 关键词：Metallosupramolecular ; Pyridinyl ; pyrimidine ; 2 ; thiol ; Crystal structure
- 刊名：Journal of Inorganic and Organometallic Polymers and Materials
- 出版年：2015
- 出版时间：March 2015
- 年：2015
- 卷：25
- 期：2
- 页码：318-326
- 全文大小：2,310 KB
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- 刊物主题：Chemistry
Inorganic Chemistry
Organic Chemistry
Polymer Sciences - 出版者：Springer New York
- ISSN：1574-1451
文摘
To explore the influence of different transition metal ions on the coordination geometries and structural architectures of metal organic complexes with flexible or semirigid tripodal ligands, [(Zn3C36H27N9S3I6)·(CHCl3)4](1), [C33H30N10S3Zn3Cl6] (2) and {[Ag2(C33H30N10S3)NO3]·NO3·H2O}n(3) were yielded by reactions of three tripodal ligands derived from pyridinyl-pyrimidine-2-thiol with ZnI2, ZnCl2 and AgNO3, respectively. The structural motifs of these complexes are multiforms from 0D to 3D interpenetrating networks. It is found that the conformational changes of ligands after interactions with metal salts are attributed to the positional isomerization of pyridine ring and effects of metal ions as well as anions. The pyridyl and pyrimidinyl rings act as N^N chelation or adopt monodentate mode in these complexes. The anions all take part in coordinating metal ions especially nitrates which can bridge silver ions to produce 1D structure in complex 3.