Coordination Behaviors and Supramolecular Interactions of 2-(2-Pyridyl) Imidazoline: Crystal Structure of Its Two Cu(II) Complexes

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• 作者：Xinmiao Wang (1)
  Chunyan Ren (1)
  Wentao Zhang (1)
  Xiang Zhou (1)
  Yang Liu (1)
  Ping Liu (1)
  Yaoyu Wang (1)
  
• 关键词：Imidazoline ; Hydrogen bond interactions ; Supramolecular
• 刊名：Journal of Inorganic and Organometallic Polymers and Materials
• 出版年：2014
• 出版时间：May 2014
• 年：2014
• 卷：24
• 期：3
• 页码：560-567
• 全文大小：2,193 KB
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• 作者单位：Xinmiao Wang (1)
  Chunyan Ren (1)
  Wentao Zhang (1)
  Xiang Zhou (1)
  Yang Liu (1)
  Ping Liu (1)
  Yaoyu Wang (1)
  
  1. Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of the Ministry of Education, Shaanxi Key Laboratory of Physico-Inorganic Chemistry, College of Chemistry & Materials Science, Northwest University, Xi’an, 710069, Shanxi, People’s Republic of China
  
• ISSN：1574-1451

文摘

Two new copper coordination complexes, [Cu(PI)(OX)(H2O)]·H2O (1) and [Cu(PI)(fum)(H2O)]·H2O (2) [PI?=?2-(2-pyridyl) imidazoline, OX2?/sup>?=?dianion of oxalic acid and fum2?/sup>?=?dianion of fumaric acid], were synthesized by interface diffusion method based on Cu(II) ions, PI ligands and aliphatic dicarboxylic acids. Complex 1 is a mononuclear complex which spreads into a 3D (4,9)-connected supramolecular network via hydrogen bond interactions, while complex 2 features a 1D zigzag chain with two different orientations. These two compounds are characterized by single crystal X-ray diffraction, powder X-ray diffraction, elemental analyses, infrared spectra, and thermogravimetric analyses.