Synthesis, solid state structures and urease inhibitory activities of two silver(I) complexes with 1,4-benzodioxane-6-carboxylate

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• 作者：Yuguang Li ; Hairui Jing ; Chengfu Ma ; Qiang Wang
• 刊名：Transition Metal Chemistry
• 出版年：2015
• 出版时间：October 2015
• 年：2015
• 卷：40
• 期：7
• 页码：743-748
• 全文大小：845 KB
• 参考文献：1.Young AG, Hanton LR (2008) Coord Chem Rev 252:1346-386CrossRef
  2.Ye?ilel OZ, Günay G, Darcan C, Soylu MS, Keskind S, Ng SW (2012) Cryst Eng Comm 14:2817-825CrossRef
  3.Wang H, Wan C, Yang J, Mak TCW (2014) Cryst Growth Des 14:3530-540CrossRef
  4.Khlobystov AN, Blake AJ, Champness NR, Lemenovskii DA, Majouga AG, Zyk NV, Schr?der M (2001) Coord Chem Rev 222:155-92CrossRef
  5.Wang Y, Englert U (2007) Eur J Inorg Chem 36:5623-625CrossRef
  6.Sun D, Cao R, Sun Y, Bi W, Li X, Wang Y, Shi Q, Li X (2003) Inorg Chem 42:7512-518CrossRef
  7.Eckhardt S, Brunetto PS, Gagnon J, Priebe M, Giese B, Fromm KM (2013) Chem Rev 113:4708-754CrossRef
  8.Chernousova S, Epple M (2013) Angew Chem Int Ed 52:1636-653CrossRef
  9.Jones SA, Bowler PG, Walker M, Parsons D (2004) Wound Repair Regen 12:288-94CrossRef
  10.Shah MSAS, Nag M, Kalagara T, Singh S, Manorama SV (2008) Chem Mater 20:2455-460CrossRef
  11.McCann M, Curran R, Ben-Shoshan M, McKee V, Tahir AA, Devereux M, Kavanagh K, Creaven BS, Kellett A (2012) Dalton Trans 41:6516-527CrossRef
  12.Coyle B, McCann M, Kavanagh K, Devereux M, McKee V, Kayal N, Egan D, Deegan C, Finn GJ (2004) J Inorg Biochem 98:1361-366CrossRef
  13.Mobley HL, Island MD, Hausinger RP (1995) Microbiol Rev 59:451-80
  14.Follmer C (2010) J Clin Pathol 63:424-30CrossRef
  15.Krajewska B (2009) J Mol Catal B Enzym 59:9-1CrossRef
  16.Vaira D, Holton J, Ricci C, Basset C, Gatta L, Perna F, Tampieri A, Miglioli M (2002) Aliment Pharmacol Ther 16:105-13CrossRef
  17.Zhu HL, Zhang XM, Liu XY, Wang XJ, Liu GF, Usman A, Fun HK (2003) Inorg Chem Commun 6:1113-116CrossRef
  18.Nomiya K, Takahashi S, Noguchi R, Nemoto S, Takayama T, Oda M (2000) Inorg Chem 39:3301-311CrossRef
  19.Kalu?erovi? MR, Gómez-Ruiz S, Gallego B, Hey-Hawkins E, Paschke R, Kalu?erovi? GN (2010) Eur J Med Chem 45:519-25CrossRef
  20.Gómez-Ruiz S, Kalu?erovi? GN, Prashar S, Hey-Hawkins E, Eri? A, ?i?ak Z, Jurani? ZD (2008) J Inorg Biochem 102:2087-096CrossRef
  21.Li X, Wang Y, Li Y, Gou Y, Wang Q (2014) Z Anorg Allg Chem 640:423-28CrossRef
  22.Sheldrick GM (2000) SMART, version 5.0. SAINT, version 6. SHELXTL, version 6.1. SADABS, version 2.03. Bruker AXS Inc., Madison
  23.Sheldrick GM (2008) Acta Crystallogr A 64:112-22CrossRef
  24.Hübschle CB, Sheldrick GM, Dittrich B (2011) J Appl Cryst 44:1281-284CrossRef
  25.Tanaka T, Kawase M, Tani S (2003) Life Sci 73:2985-990CrossRef
  26.Zaborska W, Krajewska B, Olech Z (2004) J Enzyme Inhib Med Chem 19:65-9CrossRef
  27.Van Slyke DD, Archibald RM (1944) J Biol Chem 154:623-42
  28.Nakamoto K (1997) Infrared and Raman spectra of inorganic and coordination compounds, part B: applications in coordination, organometallic, and bioinorganic chemistry. Wiley, New York
  29.Deacon GB, Phillips RJ (1980) Coord Chem Rev 33:227-50CrossRef
  30.Kole GK, Tan GK, Vittal JJ (2012) Cryst Growth Des 12:326-32CrossRef
  31.Kasuga NC, Yoshikawa R, Sakai Y, Nomiya K (2012) Inorg Chem 51:1640-647CrossRef
  32.Krajewska B (2008) J Enzyme Inhib Med Chem 23:535-42CrossRef
  33.Zaborska W, Krajewska B, Leszko M, Olech Z (2001) J Mol Catal B Enzym 13:103-08CrossRef
  
• 作者单位：Yuguang Li (1) (2)
  Hairui Jing (1)
  Chengfu Ma (1)
  Qiang Wang (1)
  
  1. School of Chemistry and Chemical Engineering, Wuhan Textile University, Wuhan, 430073, China
  2. School of Chemistry, University of Nottingham, University Park, Nottingham, NG7 2RD, UK
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Physical Chemistry
  Inorganic Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1572-901X

文摘

Two new silver(I) complexes, namely [Ag₂(BZDO)₂(H₂O)] (1) and {[Ag(bipy)(BZDO)]·[Ag(bipy)(H₂O)](BZDO)·4(H₂O)} _n (2) (BZDOH = 1,4-benzodioxane-6-carboxylic acid, bipy = 4,4-bipyridine), were synthesized and structurally characterized. Single-crystal X-ray analysis reveals that complex 1 has a discrete dinuclear silver(I) unit, [Ag₂(BZDO)₂(H₂O)], in which just one water molecule is located in the axial region and two silver atoms are further clamped by a pair of BZDO ligands in a μ ₂-em class="EmphasisTypeItalic ">η 1:η 1 bridging coordination mode (Ag···Ag = 2.8106(10) ?). Complex 2 consists of an [Ag(bipy)(BZDO)] _n chain, an [Ag(bipy)(H₂O)] _n n+ cationic chain, a one-dimensional ladder-like anionic chain formed by uncoordinated BZDO ligands and free water molecules. Both 1 and 2 show potent urease inhibitory activities with the respective IC₅₀ values of 1.60 ± 0.06 and 1.42 ± 0.09 μM. Electronic supplementary materialThe online version of this article (doi:10.-007/?s11243-015-9969-3) contains supplementary material, which is available to authorized users.