Fabrication of semiconducting pyrite thin films from hydrothermally synthesized pyrite (FeS2) powder
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- 作者：Zhengqi Shi ; Ahalapitiya H. Jayatissa…
- 刊名：Journal of Materials Science: Materials in Electronics
- 出版年：2016
- 出版时间：January 2016
- 年：2016
- 卷：27
- 期：1
- 页码：535-542
- 全文大小：3,282 KB
- 参考文献：1.A. Ennaoui, S. Fiechter, C. Pettenkofer, N. Alonso-Vante, K. Büker, M. Bronold, Ch. Höpfner, H. Tributsch, Iron disulfide for solar energy conversion. Sol. Energy Mater. Sol. Cells 29, 289–370 (1993)CrossRef
2.E.J. Kim, B. Batchelor, Synthesis and characterization of pyrite (FeS2) using microwave irradiation. Mater. Res. Bull. 44, 1553–1558 (2009)CrossRef
3.C. Wadia, Y. Wu, S. Gul, S. Volkman, J.H. Guo, A.P. Alivisatos, Surfactant-assisted hydrothermal synthesis of single phase pyrite FeS2 nanocrystals. Chem. Mater. 21, 2568–2570 (2009)CrossRef
4.I. Uhlig, R. Szargan, H.W. Nesbitt, K. Laajalehto, Surface states and reactivity of pyrite and marcasite. Appl. Surf. Sci. 179, 222–229 (2001)CrossRef
5.A. Ennaoui, S. Fiechter, W. Jaegermann, H. Tributch, Photoelectrochemistry of highly quantum efficient single-crystalline n-FeS2 (pyrite). J. Electrochem. Soc. 133(1), 97–106 (1986)CrossRef
6.B. Meester, L. Reijnen, A. Goossens, J. Schoonman, Synthesis of pyrite (FeS2) thin films by low-pressure MOCVD. Chem. Vap. Depos. 6(3), 121 (2000)CrossRef
7.J. Oertel, K. Ellmer, W. Bohne, J. Röhrich, H. Tributsch, Growth of n-type polycrystalline pyrite (FeS2) films by metalorganic chemical vapour deposition and their electrical characterization. J. Cryst. Growth 198(199), 1205–1210 (1999)CrossRef
8.N. Berry, M. Cheng, C.L. Perkins, M. Limpinsel, J.C. Hemminger, M. Law, Atmospheric-pressure chemical vapor deposition of iron pyrite thin films. Adv. Energy Mater. 2, 1124–1135 (2012)CrossRef
9.C. de las Heras, I.J. Ferrer, C. Sánchez, Pyrite thin films: improvements in their optical and electrical properties by annealing at different temperatures in a sulfur atmosphere. J. Appl. Phys. 74(7), 4551 (1993)CrossRef
10.L. Meng, Y.H. Liu, L. Tian, Structural, optical and electrical properties of polycrystalline pyrite (FeS2) films obtained by thermal sulfuration of iron films. J. Cryst. Growth 253, 530–538 (2003)CrossRef
11.N. Hamdadou, A. Khelil, J.C. Bernède, Pyrite FeS2 films obtained by sulphuration of iron pre-deposited films. Mater. Chem. Phys. 78, 591–601 (2003)CrossRef
12.R.J. Soukup, P. Prabukanthan, N.J. Ianno, A. Sarkar, C.A. Kamler, D.G. Sekora, Formation of pyrite (FeS2) thin films by thermal sulfurization of dc magnetron sputtered iron. J. Vac. Sci. Technol., A 29(1), 11001 (2011)CrossRef
13.Y.Z. Dong, Y.F. Zheng, X.G. Zhang, H. Duan, Y.F. Sun, Y.H. Chen, FeS2 (pyrite) electro-deposition thin films and study of growth mechanism. Sci. China, Ser. E Eng. Mater. Sci. 48(6), 601–611 (2005)CrossRef
14.D. Wei, K. Osseo-Asare, Aqueous synthesis of finely divided pyrite particles. Colloids Surf. A 121(1), 27–36 (1997)CrossRef
15.S. Kar, S.K. Mandal, D. Das, S. Chaudhuri, Wet chemical synthesis of iron pyrite and characterization by Mössbauer spectroscopy. Mater. Lett. 58, 2886–2889 (2004)CrossRef
16.J. Puthussery, S. Seefeld, N. Barry, M. Gibbs, M. Law, Colloidal iron pyrite (FeS2) nanocrystal inks for thin-film photovoltaics. J. Am. Chem. Soc. 133, 716–719 (2011)CrossRef
17.S.C. Hsiao, C.M. Hsu, S.Y. Chen, Y.H. Perng, Y.L. Chueh, L.J. Chen, L.H. Chou, Facile synthesis and characterization of high temperature phase FeS2 pyrite nanocrystals. Mater. Lett. 75(15), 152–154 (2012)CrossRef
18.A.M. Golsheikh, N.M. Huang, H.N. Lim, C.H. Chia, I. Harrison, M.R. Muhamad, One-pot hydrothermal synthesis and characterization of FeS2 (pyrite)/graphene nanocomposite. Chem. Eng. J. 218(15), 276–284 (2013)CrossRef
19.X.Q. Qiu, M. Liu, T. Hayashi, M. Miyauchi, K. Hashimoto, Solution-based synthesis of pyrite films with enhanced photocurrent generation. Chem. Comm. 49, 1232–1234 (2013)CrossRef
20.K.W. Sun, Z.H. Su, J. Yang, Z.L. Han, F.Y. Liu, Y.Q. Lai, J. Li, Y.X. Liu, Fabrication of pyrite FeS2 thin films by sulfurizing oxide precursor films deposited via successive ionic layer adsorption and reaction method. Thin Solid Films 542, 123–128 (2013)CrossRef
21.B. Ouertani, J. Ouerfelli, M. Saadoun, B. Bessaïs, H. Ezzaouia, J.C. Bernède, Characterization of FeS2-pyrite thin films synthesized by sulphuration of amorphous iron oxide films pre-deposited by spray pyrolysis. Mater. Charact. 54, 431–437 (2005)CrossRef
22.F. Wang, L.Y. Huang, Z.J. Luan, J.S. Huang, L. Meng, Effect of sulfurization temperature on the surface roughening, electrical and optical properties of FeS2 films deposited by sol-gel method. Mater. Chem. Phys. 132, 505–508 (2012)CrossRef
23.L. Meng, M.S. Liu, Thin pyrite (FeS2) films prepared by thermal-sulfurating iron films at various temperatures. Mater. Sci. Eng., B 60, 168–172 (1999)CrossRef
24.S. Lu, B. Panchapakesan, Photoconductivity in single wall carbon nanotube sheets. Nanotechnology 17, 1843 (2006)CrossRef - 作者单位：Zhengqi Shi (1)
Ahalapitiya H. Jayatissa (1)
Frank C. Peiris (2)
1. Nanotechnology and MEMS Laboratory, Department of Mechanical, Industrial, and Manufacturing Engineering, University of Toledo, Toledo, OH, 43606, USA
2. Department of Physics, Kenyon College, Gambier, OH, 43022, USA - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Optical and Electronic Materials
Characterization and Evaluation Materials - 出版者：Springer New York
- ISSN：1573-482X
文摘
Thin films of pyrite (FeS2) were fabricated using synthesized nano-particles and their structural, electrical and optical properties were characterized. Initially, pyrite-nano-particles were synthesized by an aqueous hydrothermal reaction. The X-ray diffraction confirmed that synthesized pyrite had a phase pure cubic pyrite structure with the average grain size around 30.0 nm. The pyrite films were fabricated by vacuum thermal evaporation of pyrite nanoparticles followed by a thermal sulfurization process. The as-deposited films have an amorphous structure and the sulfurized films have a cubic pyrite structure. The optical properties exhibited the bandgap closer to previously reported bandgap of pyrite. The photoconductivity of pyrite films was measured under AM1.5G sunlight and infrared (850 nm) light illumination. The photoconductivity data showed that the sulfurized pyrite films were more photoconductive than the as-deposited films.