Tunable double-stranded inclusion complexes of γ-cyclodextrin threaded onto non-modified poly(ethylene glycol)

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• 作者：Kai Huang ; Li Li ; Jie Wang ; Zhiming Zhou ; Xuhong Guo
• 关键词：Inclusion complex ; γ ; Cyclodextrin ; Poly(ethyl glycol) ; Double ; stranded structure
• 刊名：Colloid & Polymer Science
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：294
• 期：2
• 页码：311-319
• 全文大小：3,268 KB
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• 作者单位：Kai Huang (1)
  Li Li (1)
  Jie Wang (1)
  Zhiming Zhou (1)
  Xuhong Guo (1) (2)
  
  1. State-Key Laboratory of Chemical Engineering, East China University of Science and Technology, Shanghai, 200237, People’s Republic of China
  2. Engineering Research Center of Xinjiang Bingtuan of Materials-oriented Chemical Engineering, Shihezi University, Xinjiang, 832000, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Polymer Sciences
  Physical Chemistry
  Soft Matter and Complex Fluids
  Characterization and Evaluation Materials
  Food Science
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1435-1536

文摘

The formation of double-stranded inclusion complexes (ICs) between γ-cyclodextrin (γ-CD) and non-modified poly(ethylene glycol) (PEG) was reported to be of trace yield, while in the present work, tunable inclusion complexes between γ-CD and non-modified PEG were successfully prepared by choosing suitable γ-CD concentrations and PEG molecular weights. The obtained γ-CD/PEG ICs showed double-stranded structure whose yield, appearance, and forming rate were significantly affected by PEG molecular weight and temperature as revealed by means of optical microscopy, XRD, DSC, 1H NMR, and ITC. This improved understanding on how to control the formation of double-stranded inclusion complexes should be very helpful for preparation of more sophisticated molecular machines. Keywords Inclusion complex γ-Cyclodextrin Poly(ethyl glycol) Double-stranded structure