The fiber charge measurement depending on the poly-DADMAC accessibility to cellulose fibers

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• 作者：Hongjie Zhang ; Chengke Zhao ; Zhiqiang Li ; Jiehui Li
• 关键词：Cellulose fiber ; Fiber charge density ; Poly ; DADMAC ; Accessibility ; Polyelectrolyte adsorption
• 刊名：Cellulose
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：23
• 期：1
• 页码：163-173
• 全文大小：1,034 KB
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• 作者单位：Hongjie Zhang (1)
  Chengke Zhao (1)
  Zhiqiang Li (1)
  Jiehui Li (2)
  
  1. Tianjin Key Laboratory of Pulp and Paper, Tianjin University of Science and Technology, Tianjin, 300457, People’s Republic of China
  2. China National Pulp and Paper Research Institute, Beijing, 100102, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Bioorganic Chemistry
  Physical Chemistry
  Organic Chemistry
  Polymer Sciences
  
• 出版者：Springer Netherlands
• ISSN：1572-882X

文摘

Cellulose fiber charge is a significant parameter for porous cellulose fibers, and strongly affects the swelling ability of cellulose fibers and the properties of cellulose-based materials as well. Actually, it includes surface charge and inner charge. The surface charge is mentioned often in papermaking wet-end chemistry, however, the inner charge or the total charge is paid less attention to. In this study, the cationic polydiallyldimethyl ammonium chloride (poly-DADMAC) with different molecular weight (Mw) was applied for the accessibility evaluation to the cellulose fiber charges by using polyelectrolyte adsorption technique. Results showed that higher fiber charge was detected by lower Mw poly-DADMAC (7.5–15 kDa) due to its highly efficient penetration into the fiber cell walls and neutralization with inner charges, while lower fiber charge was obtained by using higher Mw poly-DADMAC (higher than 100 kDa) because of its adsorption onto fiber surface. As a consequence, high-Mw poly-DADMAC was used to determine the surface charge of cellulose fibers, and low-Mw poly-DADMAC could be used to measure the total charge under the saturated adsorption and low ionic strength (or salts concentration). This was confirmed by SEM–EDS analysis. The low-Mw poly-DADMAC adsorption had a good agreement with conventional conductometric titration, and a linear regression equation with slope of 1.03 and regression coefficient of 0.99 was obtained. Keywords Cellulose fiber Fiber charge density Poly-DADMAC Accessibility Polyelectrolyte adsorption