ZnO NPs: an efficient and reusable nanocatalyst for the synthesis of nitrones from DAG using H2O as a solvent at room-temperature
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- 作者：Akbar Hassanpour ; Rahim Hosseinzadeh-Khanmiri…
- 关键词：Nitrones ; Diaminoglyoxim ; Aldehyde ; Ketone ; Condensation ; ZnO NPs
- 刊名：Research on Chemical Intermediates
- 出版年：2016
- 出版时间：March 2016
- 年：2016
- 卷：42
- 期：3
- 页码：2221-2231
- 全文大小：1,015 KB
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Rahim Hosseinzadeh-Khanmiri (2)
Mirzaagha Babazadeh (2)
Laden Edjlali (2)
1. Department of Chemistry, Marand Branch, Islamic Azad University, Marand, Iran
2. Department of Chemistry, Tabriz Branch, Islamic Azad University, Tabriz, Iran - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Catalysis
Physical Chemistry
Inorganic Chemistry - 出版者：Springer Netherlands
- ISSN：1568-5675
文摘
A convenient and efficient method has been developed for the synthesis of nitrone compounds. Nitrone derivatives were synthesized in good yields via a green chemistry procedure using diaminoglyoxime and aldehyde or ketones in the presence of ZnO nanoparticles (NPs) as a catalyst in H2O as a solvent at room temperature. After the reaction course, ZnO NPs can be recycled and reused without any apparent loss of activity which makes this ecofriendly process cost effective. The structures of the compounds were characterized using IR, 1HNMR, 13CNMR and mass analysis.