Synthesis, characterization, and systematic studies of a novel aluminum selective chelating resin
详细信息 查看全文
- 作者：Aminul Islam (1)
Noushi Zaidi (1)
Hilal Ahmad (1)
Sudesh Yadav (2) - 关键词：Aluminum ; Flame atomic absorption spectrophotometer ; 2 ; (2 ; Hydroxyphenyl) benzoxazole ; Solid phase extraction
- 刊名：Environmental Monitoring and Assessment
- 出版年：2014
- 出版时间：September 2014
- 年：2014
- 卷：186
- 期：9
- 页码：5843-5853
- 全文大小：535 KB
- 参考文献：1. Abdelwahab, O. (2007). Kinetic and isotherm studies of copper(II) removal from wastewater using various adsorbents. / Egyptian Journal of Aquatic Research, 33, 125-43.
2. Bergmann, A., & Hardt, K. (1979). Analysis of dissolved Cr3+ and Cr6+ in water by APDC-MIBK extraction and atomic absorption spectrometry. / Fresenius' Zeitschrift für Analytische Chemie, 297, 381-83. CrossRef
3. Boudenne, J., Boussetta, S., Brach-Papa, C., Branger, C., Margaillan, A., & Theraulaz, F. (2002). Modification of poly(styrene-divinylbenzene) resin by grafting on an aluminium selective ligand. / Polymer International, 51, 1050-057. CrossRef
4. Carasek, E. (2000). A low-cost flame atomic absorption spectrometry method for determination of trace metals in aqueous samples. / Talanta, 51, 173-78. CrossRef
5. Chen, J., Huang, C., Hu, B., & Jiang, Z. (2004). Speciation of aluminum in drink samples by 8-hydroxyquinoline loaded silylanization silica gel microcolumn separation with off-line ICP-MS detection. / Journal of Agricultural and Food Chemistry, 52, 6843-847. CrossRef
6. Dutta, S., & Das, A. K. (2008). Separation of selected 4f and 5f metals by solid phase extraction: a review. / Journal of the Indian Chemical Society, 85, 9-1.
7. Ejaz, M., Zuha, S., Dil, W., Akhtar, A., & Chaudhri, S. A. (1981). Extraction and preconcentration of copper from water, soils, lubricating oils and plant materials and its subsequent determination by atomic absorption spectrophotometry. / Talanta, 28, 441-46. CrossRef
8. Exley, C., Merce, A. L. R., Felcman, J., & Recio, M. A. L. (2009). / Molecular and supramolecular bioinorganic chemistry. Applications in medical sciences (p. 45). New York: Nova Science Publishers Inc.
9. Erdemoglu, S. B., Pyrzyniska, K., & Gucer, S. (2000). Speciation of aluminum in tea infusion by ion-exchange resins and flame AAS detection. / Analytica Chimica Acta, 411, 81-9. CrossRef
10. Gezici, O., Kara, H., Yanik, S., Ayyildiz, H. F., & Kucukkolbasi, S. (2007). Investigating sorption characteristics of copper ions onto insolubilized humic acid by using a continuously monitored solid phase extraction technique. / Colloids Surfaces A, 298, 129-38. CrossRef
11. Horng, C. J., & Lin, S. R. (1997). Determination of urinary trace elements (As, Hg, Zn, Pb, Se) in patients with Blackfoot disease. / Talanta, 45, 75-3. CrossRef
12. Hoveyda, H. R., Rettig, S. J., & Orvig, C. (1993). Coordination chemistry of 2-(2-hydroxyphenyl)-2-benzoxazole with gallium(III) and aluminum(III): two uncommon group 13 metal environments stabilized by a biologically relevant binding group. / Inorganic Chemistry, 32, 4909-913. CrossRef
13. Henary, M. M., & Fahrni, C. J. (2002). Excited state intramolecular proton transfer and metal ion complexation of 2-(2-hydroxyphenyl) benzazoles in aqueous solution. / Journal of Physical Chemistry A, 106, 5210-220. CrossRef
14. Islam, A., Ahmad, A., & Laskar, M. A. (2011a). A newly developed salicylanilide functionalized amberlite XAD-16 chelating resin for use in preconcentration and determination of trace metal ions from environmental and biological samples. / Analytical Methods, 3, 2041-048. CrossRef
15. Islam, A., Ahmad, A., & Laskar, M. A. (2012a). Preparation, characterization of a novel chelating resin functionalized with / o-hydroxybenzamide and its application for preconcentration of trace metal ions. / Clean - Soil, Air, Water, 40, 54-5. CrossRef
16. Islam, A., Ahmad, A., & Laskar, M. A. (2012b). Characterization of a chelating resin functionalized via azo spacer and its analytical applicability for the determination of trace metal ions in real matrices. / Journal of Applied Polymer Science, 123, 3448-458. CrossRef
17. Islam, A., Laskar, M. A., & Ahmad, A. (2011b). The efficiency of amberlite XAD-4 resin loaded with 1-(2-pyridylazo)-2-naphthol in preconcentration and separation of some toxic metal ions by flame atomic absorption spectrometry. / Environmental Monitoring and Assessment, 175, 201-12. CrossRef
18. Islam, A., Laskar, M. A., & Ahmad, A. (2013a). Preconcentration of metal ions through chelation on a synthesized resin containing O, O donor atoms for quantitative analysis of environmental and biological samples. / Environmental Monitoring and Assessment, 185, 2691-704. CrossRef
19. Islam, A., Laskar, M. A., & Ahmad, A. (2010a). Characterization and application of 1-(2-pyridylazo)-2-naphthol functionalized amberlite XAD-4 for preconcentration of trace metal ions in real matrices. / Journal of Chemical and Engineering Data, 55, 5553-561. CrossRef
20. Islam, A., Laskar, M. A., & Ahmad, A. (2010b). Characterization of a novel chelating resin of enhanced hydrophilicity and its analytical utility for preconcentration of trace metal ions. / Talanta, 81, 1772-780. CrossRef
21. Islam, A., Ahmad, H., Zaidi, N., & Yadav, S. (2013b). Selective separation of aluminum from biological and environmental samples using glyoxal-bis(2-hydroxyanil) functionalized amberlite XAD-16 resin: kinetics and equilibrium studies. / Industrial and Engineering Chemistry Research, 52, 5213-220. CrossRef
22. Langmuir, I. (1918). The sorption of gases on plane surfaces of glass, mica and platinum. / Journal of the American Chemical Society, 40, 1361-403. CrossRef
23. Long, G. L., & Winefordner, J. D. (1983). Limit of detection: a closer look at the IUPAC definition. / Analytical Chemistry, 55, 712A-24A. CrossRef
24. Luo, M., & Bi, S. (2003). Solid phase extraction-spectrophotometric determination of dissolved aluminum in soil extracts and ground waters. / Journal of Inorganic Biochemistry, 97, 173-78. CrossRef
25. Matus, P., & Kubova, J. (2006). Complexation efficiency of differently fixed 8-hydroxyquinoline and salicylic acid ligand groups for labile aluminium species determination in soils-comparison of two methods. / Analytica Chimica Acta, 573-74, 474-81. CrossRef
26. Mizuike, A. (1983). / Enrichment techniques for inorganic trace analysis. Berlin: Springer. CrossRef
27. Martin-Esteban, A., Fernandez, P., Perez-Conde, C., Gutierrez, A., & Camara, C. (1995). On-line preconcentration of aluminium with immobilized Chromotrope 2B for the determination by flame atomic absorption spectrometry and inductively coupled plasma mass spectrometry. / Analytica Chimica Acta, 304, 121-26. CrossRef
28. Mohammad, B., Ure, A. M., & Littlejohn, D. (1992). On-line preconcentration of aluminium with immobilized 8-hydroxyquinoline for determination by atomic absorption spectrometry. / Journal of Analytical Atomic Spectrometry, 7, 695-99. CrossRef
29. Neal, C., Rowland, P., Neal, M., Jarvie, H. P., Lawlor, A., Sleep, D., & Scholefield, P. (2011). Aluminium in UK rivers: a need for integrated research related to kinetic factors, colloidal transport, carbon and habitat. / Journal of Environmental Monitoring, 13, 2153-162. CrossRef
30. Ottaway, J. M., & Pradhan, N. K. (1973). Determination of chromium in steel by atomic absorption spectrometry with an air acetylene flame. / Talanta, 20, 927-31. CrossRef
31. Paleologos, E. K., Giokas, D. L., & Karayannis, M. I. (2005). Micelle-mediated separation and cloud-point extraction. / Trends in Analytical Chemistry, 24, 426-36. CrossRef
32. Popova, S. A., Bratinova, S. P., & Ivanova, C. R. (1991). Determination of trace amounts of copper, nickel and zinc in palladium compounds by solvent extraction flame atomic absorption spectrometry. / Analyst, 116, 525-31. CrossRef
33. Pearson, R. G. (1968). Hard and soft acids and bases, HSAB, Part II. / Journal of Chemical Education, 45, 643-48. CrossRef
34. Pearson, R. G. (1963). Hard and soft acids and bases. / Journal of the American Chemical Society, 84, 3533-539. CrossRef
35. Pyrzynska, K., & Trojanowicz, M. (1999). Functionalized cellulose sorbents for preconcentration of trace metals in environmental analysis. / Critical Reviews in Analytical Chemistry, 29, 313-21. CrossRef
36. Pesavento, M., Biesuz, R., Alberti, G., & Sturini, M. (2003). Separation of copper(II) and aluminium(III) from fresh waters by solid phase extraction on a complexing resin column. / Journal of Separation Science, 26, 381-86. CrossRef
37. Qin, W., Obare, S. O., Murphy, C. J., & Angel, S. M. (2001). Specific fluorescence determination of lithium ion based on 2-(2-hydroxyphenyl)benzoxazole. / Analyst, 126, 1499-501. CrossRef
38. Resing, J. A., & Measures, C. I. (1994). Fluorometric determination of Al in seawater by flow injection analysis with in-line preconcentration. / Analytical Chemistry, 66, 4105-111. CrossRef
39. Silva, E. L., Grauzarolli, E. M., & Carasek, E. (2004). Use of Nb2O5-SiO2 in an automated on-line preconcentration system for determination of copper and cadmium by FAAS. / Talanta, 62, 727-33. CrossRef
40. Saxena, R., & Singh, A. K. (1997). Pyrocatechol violet immobilized Amberlite XAD-2: synthesis and metal-ion uptake properties suitable for analytical applications. / Analytica Chimica Acta, 340, 285-90. CrossRef
41. Sombra, L. L., Wuilloud, R. G., Olsina, R. A., Fernandez, L. P., & Martinez, L. D. (2000). On-line preconcentration system for aluminum determination in parenteral solutions using flow injection-inductively coupled plasma atomic emission spectrometry. / Journal of Trace and Microprobe Techniques, 18, 431-36.
42. Tian, Y., Chen, C. Y., Yang, C. C., Young, A. C., Jang, S. H., Chen, W. C., & Jen, A. K. Y. (2008). 2-(2-Hydroxyphenyl)benzoxazole-containing two-photon-absorbing chromophores as sensors for zinc and hydroxide ions. / Chemistry of Materials, 20, 1977-987. CrossRef
43. Welcher, F. J. (1958). / The analytical uses of ethylenediaminetetraacetic acid. New York: Van Nostrand Company.
44. Yuan, D., & Shuttler, I. L. (1995). Flow-injection column preconcentration directly coupled with electrothermal atomization atomic absorption spectrometry for the determination of aluminium. Comparison of column packing materials. / Analytica Chimica Acta, 316, 313-22. CrossRef
45. Yaman, M. (2001). Simultaneous enrichment of Cd, Pb, Ni and Al and their determination in water by STAT-FAAS. / Spectroscopy Letters, 34, 763-68. CrossRef
46. Zhang, X. B., Peng, J., He, C. L., Shen, G. L., & Yu, R. Q. (2006). A highly selective fluorescent sensor for Cu2+ based on 2-(2-hydroxyphenyl)benzoxazole in a poly(vinyl chloride) matrix. / Analytica Chimica Acta, 567, 189-95. CrossRef - 作者单位：Aminul Islam (1)
Noushi Zaidi (1)
Hilal Ahmad (1)
Sudesh Yadav (2)
1. Analytical Research Laboratory, Department of Chemistry, Aligarh Muslim University, Aligarh, 202002, India
2. School of Environmental Sciences, Jawaharlal Nehru University, New Mehrauli Road, New Delhi, 110067, India - ISSN：1573-2959
文摘
A procedure is detailed for the selective analysis of trace aluminum by flame atomic absorption spectrophotometer coupled with off-line column separation and preconcentration. Chelating resin was synthesized by covalent functionalization of Amberlite XAD-16 by 2-(2-hydroxyphenyl) benzoxazole. The modified resin was characterized using FT-IR spectroscopy, energy dispersive x-ray analysis, elemental analysis, thermogravimetric analysis/differential thermal analysis, and minimum energy run. The optimum sorption was at pH?9?±-.1 with corresponding t 1/2 of only 7?min. Many competitive anions and cations studied did not interfere at all in the selective determination of Al(III), at the optimized conditions. The resin shows maximum sorption capacity of 21.58?mg?g? and can be regenerated up to 75?cycles without any discernible capacity loss. The Langmuir isotherm model provides the better correlation of the experimental data (r 2--.999) in comparison to Freundlich isotherm model, while the Scatchard analysis revealed homogeneous binding sites in the chelating resin. Analytical figures of merit were evaluated by accuracy (standard reference materials and recovery experiment), precision (RSD ?). The applicability was demonstrated by analysis of trace aluminum in biological, environmental, and food samples.