Three Novel Cd(II) and Zn(II) Coordination Polymers with O-, N-donor Ligands: Syntheses, Structures, and Photoluminescence Properties
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- 作者：Yong-Hong Zhou
- 关键词：Coordination polymer ; N ; donor ligand ; Crystal structure ; Luminescence ; Cadmium(II) complex ; Zinc(II) complex
- 刊名：Journal of Inorganic and Organometallic Polymers and Materials
- 出版年：2015
- 出版时间：May 2015
- 年：2015
- 卷：25
- 期：3
- 页码：535-543
- 全文大小：2,376 KB
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1. School of Chemistry and Material Science, Huaibei Normal University, Huaibei, 235000, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Inorganic Chemistry
Organic Chemistry
Polymer Sciences - 出版者：Springer New York
- ISSN：1574-1451
文摘
Three new multi-dimensional coordination polymers, namely, [Cd(SIP)(HBPP)(BPP)0.5(H2O)·H2O]n (1), [Zn(L)(BIB)0.5]n (2), and {[Cd2(L)2(BIB)2](H2O)7}n (3) (H3SIP?=?5-sulfo-1,3-benzenedicarboxylate, BPP?=?1,3-bis(4-pyridyl)propane, H2L?=?4-oxyacetate-benzoic acid, and BIB?=?1,4-bis(imidazol-1-yl)-butane), were hydrothermally synthesized by self-assembly of the flexible N-donor ligand and the polycarboxylate ligands. Single crystal X-ray analyses reveal that complexes 1-strong class="EmphasisTypeBold">3 possess different structural features. The Cd(II) atom in complex 1 is seven-coordinated by two bidentate chelating carboxylate groups and two nitrogen atoms as well as one water molecule. The adjacent Cd(II) atoms are bridged by two carboxylate groups to form 1D chains running along different directions, which are connected by BPP ligands to generate 2D network. The resulting 2D networks are further linked by hydrogen-bond interactions, affording a 3D supramolecular architecture. In complex 2, the [Zn2(COO)4] units are bridged by L2?/sup> ligands to generate 1D double chain structure and then linked by BIB ligands to give 2D grid framework. In complex 3, the [Cd(L2)]n and [Cd(BIB)]n helixes are alternately arranged, leading to the formation of a 2D bilayer structure.