Synthesis and properties of functionalized Schiff bases of 5α,10α-di(4-hydroxylphenyl)calix[4]pyrrole and 5α,15β-di(4-hydroxylphenyl)c
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- 作者：Ying Han (1)
Juanjuan Sun (1)
Genliang Wang (1)
Chaoguo Yan (1) - 关键词：Calix[4]pyrrole ; Schiff base ; Macrocycle ; Crystal structure ; UV ; Vis spectroscopy
- 刊名：Chemical Research in Chinese Universities
- 出版年：2014
- 出版时间：December 2014
- 年：2014
- 卷：30
- 期：6
- 页码：919-924
- 全文大小：612 KB
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Chaoguo Yan (1)
1. College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, 225002, P. R. China - ISSN：2210-3171
文摘
A series of calix[4]pyrrole meso-substituted Schiff bases was synthesized with 5α,10α-di(4-hydroxylphenyl)calix[4]pyrrole or 5α,15β-di(4-hydroxylphenyl)calix[4]pyrrole as starting material. The synthetic routes included alkylation with methyl α-chlroroaceate, ammonolysis with alkylene diamine, and condensation with salicylladehyde or 2-hydroxynaphthaldehyde. The crystal structures of the new calix[4]pyrroles and their Schiff bases were determined by X-ray diffraction. The coordination properties of the representative calix[4]pyrrole Schiff bases to transition metal ions were also investigated by UV-Vis spectra.