A Highly Sensitive and Selective Spectrofluorimetric Method for the Determination of Nitrite in Food Products

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• 作者：Qiuhua Wang ; Haiwei Huang ; Baoming Ning ; Minfeng Li ; Lan He
• 关键词：Nitrite ; Spectrofluorimetric ; Determination ; 4 ; Amino ; 5 ; methylamino ; 2′ ; 7′-difluorofluorescein diacetate (DAF ; FM DA)
• 刊名：Food Analytical Methods
• 出版年：2016
• 出版时间：May 2016
• 年：2016
• 卷：9
• 期：5
• 页码：1293-1300
• 全文大小：398 KB
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• 作者单位：Qiuhua Wang (1) (2)
  Haiwei Huang (1)
  Baoming Ning (1)
  Minfeng Li (2)
  Lan He (1)
  
  1. National Institutes for Food and Drug Control, Beijing, 100050, China
  2. College of Chemistry, Beijing Normal University, Beijing, 100875, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

This paper describes a simple, sensitive, and selective spectrofluorimetric method to determine trace amount of nitrite in food products using 4-amino-5-methylamino-2′,7′-difluorofluorescein diacetate (DAF-FM DA) as a fluorescent probe. The reaction of DAF-FM DA with nitrite in acidic medium resulted in triazolofluorescein (DAF-FM T), a highly fluorescent reagent in neutral medium. The fluorescence enhancement was proportional to nitrite concentration in the range of 5.0 × 10−8 to 1.5 × 10−6 mol L−1 with a detection limit of 3.3 × 10−8 mol L−1 (S/N = 3). The proposed method has been applied to the determination of nitrite in real food samples, with relative standard deviation (RSD) (n = 6) less than 5.1 % and recoveries in the range of 86.4 ~ 102.9 %.