Effects of surface residual species in SBA-16 on encapsulated chiral (1S,2S)-DPEN-RuCl2(TPP)2 in asymmetric hydrogenation of acetophenone

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• 作者：Xiufeng Shi ; Bin Xing ; Binbin Fan ; Zhaoteng Xue…
• 关键词：template residuals ; mesoporous silicas ; chiral Ru complex ; asymmetric hydrogenation ; acetophenone
• 刊名：Russian Journal of Physical Chemistry A, Focus on Chemistry
• 出版年：2016
• 出版时间：March 2016
• 年：2016
• 卷：90
• 期：3
• 页码：545-551
• 全文大小：437 KB
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• 作者单位：Xiufeng Shi (1)
  Bin Xing (1)
  Binbin Fan (1)
  Zhaoteng Xue (2)
  Ruifeng Li (1)
  
  1. College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan, 030024, China
  2. Department of Chemistry and Shanghai Key Laboratory of Molecular Catalysis and Innovative Materials, Laboratory of Advanced Materials, Fudan University, Shanghai, 200433, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Physical Chemistry
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1531-863X

文摘

The SBA-16 obtained by different routes of elimination of organic templates were used as the hosts for encapsulation of chiral Ru complex (1S,2S)-DPEN-RuCl₂(TPP)₂ (1) (DPEN = 1,2-diphenylethylene-diamine, TPP = triphenyl phosphine). The methods for removing templates had distinct effects on the amount of residual template in SBA-16, which made the SBA-16 with different surface and structure properties. 1 encapsulated in SBA-16 extracted with the mixture of pyridine and ethanol showed higher activity and enantioselectivity for acetophenone asymmetric hydrogenation.