Synthesis of graphene oxide-wrapped core–shell structured carbon sphere@Al2O3 as electrode material for voltammetric determination of butylated hydroxyanisole in food products

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• 作者：Tian Gan ; Zhaoxia Shi ; Danyang Hu ; Junyong Sun ; Haibo Wang ; Yanming Liu
• 关键词：Al2O3 ; Carbon sphere ; Graphene oxide ; Butylated hydroxyanisole ; Electrochemical determination
• 刊名：Ionics
• 出版年：2015
• 出版时间：October 2015
• 年：2015
• 卷：21
• 期：10
• 页码：2959-2968
• 全文大小：1,303 KB
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• 作者单位：Tian Gan (1)
  Zhaoxia Shi (1)
  Danyang Hu (1)
  Junyong Sun (1)
  Haibo Wang (1)
  Yanming Liu (1)
  
  1. College of Chemistry and Chemical Engineering, Xinyang Normal University, Xinyang, 464000, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Electrochemistry
  Materials Science
  Physical Chemistry
  Condensed Matter
  Renewable Energy Sources
  Electrical Power Generation and Transmission
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1862-0760

文摘

Here, we report a graphene oxide-wrapped core–shell structured carbon sphere@Al₂O₃ composite (CS@Al₂O₃@GO) as the electrode material for sensitive determination of butylated hydroxyanisole (BHA). The core–shell structured CS@Al₂O₃ was synthesized through a solution-based approach by using glucose and metal salts as precursors via a simple one-pot hydrothermal synthesis. Then, the CS@Al₂O₃ was amino-functionalized and wrapped by conductive graphene oxide (GO) sheets through the electrostatic interaction. As a result, the CS@Al₂O₃@GO endowed the modified electrode fast electron transfer rate and high electrocatalytic activity toward BHA oxidation. Under the optimal conditions, the oxidation current increased linearly with the concentration of BHA in the range of 0.2~200 μM with the detection limit and quantification limit of 41 and 136.7 nM using differential pulse voltammetry. The presented method was also demonstrated for the determination of BHA in food samples with satisfactory results. Keywords Al₂O₃ Carbon sphere Graphene oxide Butylated hydroxyanisole Electrochemical determination