Effect of coupling agents and ionic liquid on the properties of rice bran carbon/carboxylated styrene butadiene rubber composites

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• 作者：Yinhang Zhang ; Xiangxu Li ; Xin Ge ; Fei Deng ; Ur Ryong Cho
• 关键词：coupling agents ; ionic liquid ; carboxylated styrene butadiene rubber ; composites ; latex compounding method
• 刊名：Macromolecular Research
• 出版年：2015
• 出版时间：October 2015
• 年：2015
• 卷：23
• 期：10
• 页码：952-959
• 全文大小：613 KB
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• 作者单位：Yinhang Zhang (1)
  Xiangxu Li (1)
  Xin Ge (1)
  Fei Deng (1)
  Ur Ryong Cho (1)
  
  1. School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education, Cheonan, Chungnam, 330-708, Korea
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Physical Chemistry
  Polymer Sciences
  Characterization and Evaluation of Materials
  Soft and Granular Matter, Complex Fluids and Microfluidics
  Nanochemistry
  Nanotec
  
• 出版者：The Polymer Society of Korea, co-published with Springer
• ISSN：2092-7673

文摘

Latex compounding method (LCM) was applied to ensure a better dispersion state of filler in rubber matrix. In order to enhance the compatibility and interfacial interaction between carboxylated-styrene butadiene rubber (XSBR) and rice bran carbon (RBC), a series of coupling agents i.e., N-(2-aminoethyl)-3-aminopropyltrimethoxysilane (AAPTS), 3-mercaptopropyltrimethoxysilane (MPTMS), 4,4-methylene bis(phenyl isocyanate) (MDI) and ionic liquid 1-hexyl-3-methylimidazolium hexafluorophosphate (HMIMPF6) were applied. Morphology of the fracture surface, mechanical property, thermal stability, vulcanization characters and dynamic mechanical property were investigated. The characterization on the resultant composites demonstrated that the MDI exhibited the superior reinforcing effect, of which the tensile strength and 300% modulus reached to 16.43 and 16.33 MPa, respectively. The study on fracture surface, Raman spectrum, thermal stability and storage modulus confirmed the strong interfacial interaction resulted from MDI. In addition, ionic liquid also exhibited coupling activity, improving the mechanical properties of the composites.