Surface-imprinted magnetic particles for highly selective sulfonamides recognition prepared by reversible addition fragmentation chain transfer polymerization

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• 作者：Xiaoyu Xie ; Xia Liu ; Xiaoyan Pan ; Liang Chen…
• 关键词：Molecularly imprinted polymers ; Super paramagnetic ; Reversible addition fragmentation chain transfer polymerization ; Sulfonamides
• 刊名：Analytical and Bioanalytical Chemistry
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：408
• 期：3
• 页码：963-970
• 全文大小：775 KB
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• 作者单位：Xiaoyu Xie (1)
  Xia Liu (1)
  Xiaoyan Pan (1)
  Liang Chen (1)
  Sicen Wang (1)
  
  1. School of Pharmacy, Health Science Center, Xi’an Jiaotong University, 710061, Xi’an, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Food Science
  Inorganic Chemistry
  Physical Chemistry
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1618-2650

文摘

In this work, novel magnetic molecularly imprinted polymers (MMIPs) were prepared by reversible addition fragmentation chain transfer (RAFT) polymerization using sulfamerazine as the template. With the controlled/living property of RAFT polymerization, the resulting MMIPs showed high selectivity for sulfonamides recognition. The MMIPs were characterized by transmission electron microscopy, Fourier transform infrared, vibrating sample magnetometer, X-ray diffraction, X-ray photoelectron spectroscopy, and thermogravimetric analysis. The static and selectivity binding experiments demonstrated the desirable adsorption capacity and high selectivity of the MMIPs. The developed MMIPs were used as the solid-phase extraction sorbents to selectively extract four sulfonamides from aqueous solution. The recoveries of the spiked pond water ranged from 61.2 to 94.1 % with RSD lower than 6.5 %. This work demonstrated a versatile approach for the preparation of well-constructed MMIPs for application in the field of solid-phase extraction.