Nanomagnetically modified polyphosphoric acid (NiFe2O4@SiO2–PPA): an efficient, fast, and reusable catalyst for the synthesis of 2-thioxoquinazolinones under s
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  • 作者:Hossein Eshghi ; Amir Khojastehnezhad ; Farid Moeinpour…
  • 关键词:Polyphosphoric acid ; Magnetic nanoparticles ; One ; pot ; three ; component ; 2 ; Thioxoquinazolinones ; Isatoic anhydride
  • 刊名:Research on Chemical Intermediates
  • 出版年:2015
  • 出版时间:October 2015
  • 年:2015
  • 卷:41
  • 期:10
  • 页码:7915-7924
  • 全文大小:1,289 KB
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  • 作者单位:Hossein Eshghi (1)
    Amir Khojastehnezhad (2)
    Farid Moeinpour (3)
    Mehdi Bakavoli (1)
    Nafiseh Zeinabi (2)
    Sadegh Allameh (2)

    1. Department of Chemistry, Faculty of Sciences, Ferdowsi University of Mashhad, Mashhad, Iran
    2. Department of Chemistry, College of Science, Islamic Azad University, Mashhad Branch, Mashhad, Iran
    3. Department of Chemistry, College of Science, Islamic Azad University, Bandar Abbas Branch, 7915893144, Bandar Abbas, Iran
  • 刊物类别:Chemistry and Materials Science
  • 刊物主题:Chemistry
    Catalysis
    Physical Chemistry
    Inorganic Chemistry
  • 出版者:Springer Netherlands
  • ISSN:1568-5675
文摘
Polyphosphoric acid functionalized silica-coated magnetic nanoparticles with core–shell structure (NiFe2O4@SiO2–PPA) has been used as a magnetically recyclable green catalyst for the one-pot three-component synthesis of 2-thioxoquinazolinones by the reaction of isatoic anhydride, primary amines and thiourea under neat conditions. The catalyst is readily recovered by simple magnetic decantation and can be recycled five times with no significant loss of catalytic activity. Keywords Polyphosphoric acid Magnetic nanoparticles One-pot, three-component 2-Thioxoquinazolinones Isatoic anhydride

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