Reactive sintering of (K0.5Bi0.5)TiO3-BiFeO3 lead-free piezoelectric ceramics

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• 作者：John G. Fisher ; Min-Gu Kim ; Daeung Kim…
• 关键词：Lead ; free piezoelectric ; BiFeO3 ; Reactive sintering ; Dielectric properties ; Piezoelectric properties ; MnO ; doping
• 刊名：Journal of the Korean Physical Society
• 出版年：2015
• 出版时间：May 2015
• 年：2015
• 卷：66
• 期：9
• 页码：1426-1438
• 全文大小：2,841 KB
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• 作者单位：John G. Fisher (1)
  Min-Gu Kim (1)
  Daeung Kim (1)
  Su-Jeong Cha (1)
  Hung Van Vu (1)
  Dieu Nguyen (1)
  Young-Hun Kim (1)
  Su-Hyun Moon (1)
  Jong-Sook Lee (1)
  Ali Hussain (2)
  Myong-Ho Kim (2)
  
  1. School of Materials Science and Engineering, Chonnam National University, Gwangju, 500-757, Korea
  2. School of Nano & Advanced Materials Engineering, Changwon National University, Changwon, 641-773, Korea
  
• 刊物主题：Physics, general; Theoretical, Mathematical and Computational Physics; Particle and Nuclear Physics;
• 出版者：Springer Netherlands
• ISSN：1976-8524

文摘

Ceramics based on BiFeO₃ are potential lead-free replacements for Pb(Zr,Ti)O₃ in a variety of applications such as sensors, transducers and actuators. Recently, ceramics in the (K_0.5Bi_0.5)TiO₃-BiFeO₃ system were developed which have excellent piezoelectric properties. However, these ceramics are difficult to sinter to high density. The present work studies the use of reactive sintering to prepare 0.4(K_0.5Bi_0.5)TiO₃-0.6BiFeO₃ ceramics. Undoped and MnO-doped powders were prepared by ball milling K₂CO₃, (BiO)₂CO₃, TiO₂, α-FeO(OH) and MnCO₃ in ethanol with zirconia milling media. The decomposition and calcination reactions of the starting materials were studied using differential scanning calorimetry/thermogravimetric analysis, X-ray diffraction and Fourier transform infra-red analysis. Samples were sintered in the temperature range from 1000 to 1075°C and their structures and microstructures examined using X-ray diffraction, micro-Raman scattering and scanning electron microscopy. MnO doping reduced the rhombohedral distortion of the unit cell. The dielectric, ferroelectric and piezoelectric properties of selected undoped and MnO-doped samples were measured. Both undoped and MnO-doped samples displayed relaxor-type behavior. MnO doping reduced the conductivity of the samples, which exhibit a well-defined activation energy of 1.21 eV. Undoped samples have strain vs. electric field properties comparable to those reported in the literature.