Microwave synthesis of nanosized particles of a complex oxide system with a garnet structure

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• 作者：O. G. Klimova ; I. A. Sizova ; V. V. Galkin ; A. V. Makeenko…
• 刊名：Glass Physics and Chemistry
• 出版年：2016
• 出版时间：July 2016
• 年：2016
• 卷：42
• 期：4
• 页码：403-407
• 全文大小：516 KB
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Ceramics,Glass,Composites,Natural Materials
  Characterization and Evaluation Materials
  Materials Science
  Physical Chemistry
  Russian Library of Science
  
• 出版者：MAIK Nauka/Interperiodica distributed exclusively by Springer Science+Business Media LLC.
• ISSN：1608-313X
• 卷排序：42

文摘

The possibility of applying the method of microwave synthesis for the fabrication of nanosized particles of complex oxides has been demonstrated. The effect of fabrication conditions on the size of nanoparticles with a garnet structure has been established on the example of the Gd–Ga–Al–O system. The concentration of the organic solvent for obtaining particles of an average size of 50 nm has been determined experimentally. The phase composition of thermally treated samples has been investigated. The optimal conditions of producing nanosized powders of garnets, Gd₃(Ga,Al)₅O₁₂, have been determined.Keywordsceramic materialsgarnetcomplex oxidesnanoparticlesmicrowave synthesispolyol synthesis