Simultaneous determination of ascorbic acid, dopamine and uric acid using a glassy carbon electrode modified with the nickel(II)-bis(1,10-phenanthroline) complex and single-walled carbon nanotubes
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- 作者：Songling Yan ; Xi Li ; Yan Xiong ; Mengmeng Wang ; Linlin Yang ; Xin Liu…
- 关键词：Nanomaterial ; Scanning electron microscopy ; Cylic voltammetry ; Electrochemical impedance spectroscopy ; Pharmaceutical analysis ; Urine analysis
- 刊名：Microchimica Acta
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：183
- 期：4
- 页码：1401-1408
- 全文大小：580 KB
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Xi Li (1)
Yan Xiong (1)
Mengmeng Wang (1)
Linlin Yang (1)
Xin Liu (1)
Xiaoyu Li (1)
Lina Abdullah M Alshahrani (1)
Peng Liu (1)
Chaocan Zhang (2)
1. Department of Chemistry, School of Science, Wuhan University of Technology, Wuhan, 430070, People’s Republic of China
2. School of Materials Science and Engineering, Wuhan University of Technology, Wuhan, 430070, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Analytical Chemistry
Inorganic Chemistry
Physical Chemistry
Characterization and Evaluation Materials
Monitoring, Environmental Analysis and Environmental Ecotoxicology - 出版者：Springer Wien
- ISSN：1436-5073
文摘
The authors report that a glassy carbon electrode modified with the [Ni(phen)2]2+ complex and single-walled carbon nanotubes represents a useful sensor for simultaneous determination of ascorbic acid (AA), dopamine (DA) and uric acid (UA). The material was characterized by scanning electron microscopy, and the electrode by cyclic voltammetry and electrochemical impedance spectroscopy. The experiments showed that this electrode responds to AA, DA and UA, best at working potentials of 0.130 V, 0.334 V, 0.486 V (vs. SCE), over the wide linear ranges from 30 to 1546 μM (for AA), 1 to 780 μM (for DA), and 1 to 1407 μM (for UA). The respective detection limits are 12 μM, 1 μM and 0.76 μM at an S/N ratio of 3. The modified electrode was successfully applied to the determination of AA, DA and UA in real samples.