Elastic behaviour of microwave hydrothermally synthesized nanocrystalline Mn_{1鈭?span style='font-style: italic'>x}-Zn_x ferrites

详细信息	查看全文 | 推荐本文 |

• 作者：K. Praveena ; ^{praveenaou@gmail.com} ; K. Sadhana ; S.R. Murthy
• 关键词：A. Nanocrystalline ferrites ; B. Microwave-Hydrothermal method ; C. Microwave annealing ; D. Elastic properties
• 刊名：Materials Research Bulletin
• 出版年：2012
• 期刊代码：60_00255408
• 类别：ms
• 出版时间：April, 2012
• 卷：47
• 期：4
• 页码：1096-1103
• 文件大小：1366 K

摘要

Microwave-hydrothermal (M-H) method has been successfully used for synthesis of nanocrystalline Mn-Zn ferrites which are used for high frequency applications. The nanopowders were characterized using XRD and TEM. The particle size of the samples varies from 鈭?0 nm to 25 nm. The powders were densified at 900 掳C/30 min using microwave sintering method. The sintered ferrite samples were characterized using XRD, X-ray photoelectron spectroscopy (XPS), SEM and energy dispersive X-ray spectroscopy (EDS). The elastic behaviour and internal friction studies were carried out using composite piezoelectric oscillator method in the temperature range of 300-600 K. It was found that the anomalous behaviour observed in the temperature dependence of Young's modulus and internal friction disappears with the application of a magnetic field equal to the saturation field (900 mT) of the specimen under investigation. The observed anomalous behaviour in the vicinity of the Curie temperature was understood with the help of Landau's theory.