The metallographic and X-ray diffraction data are given for the new ternary silicide U3MoSi2. This compound melts incongruently at approximately 1480°C according to: U3MoSi2→U4MoSi3 + U2Mo3Si4 + L (L=peritectic liquid). It was verified that molybdenum coexists with U3Si2 predominantly as U3MoSi2. Indexing of the powder pattern showed that U3MoSi2 has a simple cubic structure with lattice parameter a0=10.69 ± 0.01 Å.