Synthesis and characterisation of a new vanadyl oxalatophosphate compound: (C₁₀H₁₀N₂)[(VO)(HPO₄)]₂(C₂O₄)

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• 作者：Shi ; Fa-Nian ; Almeida Paz ; Filipe A. ; Rocha ; Jo脙脙o ; Klinowski ; Jacek ; Trindade ; Tito
• 关键词：Vanadyl oxolatophosphate ; Hybrid material ; Crystal structure
• 刊名：Inorganica Chimica Acta
• 出版年：2005
• 期刊代码：40_00201693
• 类别：ch
• 出版时间：March 1, 2005
• 卷：358
• 期：4
• 页码：927-932
• 文件大小：842 K

摘要

A new vanadyl oxalatophosphate compound, (C₁₀H₁₀N₂)[(VO)(HPO₄)]₂(C₂O₄), was synthesized via the hydrothermal approach and characterised structurally using single-crystal X-ray diffraction, FT-IR and thermogravimetric analysis. The compound has two-dimensional Formula Not Shown anionic layers with Formula Not Shown occupying the interlayer spaces.