Optimization of conditions of solvent-free microwave extraction and study on antioxidant capacity of essential oil from Schisandra chinensis (Turcz.) Baill

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• 作者：Chun-hui Ma¹ ; Lei Yang ; ¹ ; ^{zygorl@126.com} ; ^{ylmanefu@163.com} ; Yuan-gang Zu ; Ting-ting Liu
• 关键词：Schisandra chinensis (Turcz.) Baill. (S. chinensis) ; Solvent-free microwave extraction (SFME) ; Central composite design (CCD) ; Hydro-distillation (HD) ; Steam-distillation (SD)
• 刊名：Food Chemistry
• 出版年：2012
• 期刊代码：48_03088146
• 类别：abs
• 出版时间：15 October, 2012
• 卷：134
• 期：4
• 页码：2532-2539
• 文件大小：554 K

摘要

In this article, solvent-free microwave extraction (SFME) of essential oil from Schisandra chinensis (Turcz.) Baill was studied. A multivariate study based on central composite design (CCD) was used to evaluate the influence of three major variables affecting the performance of SFME. The optimum parameters were extraction time 30 min, irradiation power 385 W and moisture content of the fruits was 68%. The extraction yield of essential oil was 11 ml/kg under the optimum conditions. The antioxidant capacity of essential oils extracted by different methods were determined, and compared with traditional antioxidants. GC-MS showed the different composition of essential oil extracted by hydro-distillation (HD), steam-distillation (SD) and SFME. S. chinensis materials treated by different methods were observed by scanning electronic microscopy (SEM) and thermo-gravimetric analysis (TGA). Micrographs and thermo gravimetric loss provided more evidences to prove SFME of essential oil is more completed than HD and SD.